用降压法合成沙质镁铁

Cahyo Saputra, Heru Cahyoutomo, Jeny Sendong, Octolia Togibasa
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引用次数: 0

摘要

以天然铁砂为原料,采用共沉淀法合成了铁酸镁。铁砂材料取自巴布亚省萨尔米摄政北部海岸。本研究的目的是研究是否可以直接从铁砂中合成铁酸镁,而不需要预处理。采用共沉淀法,搅拌温度分别为30、50、70℃。用x射线衍射仪对晶体结构进行表征,用振动样品磁强计对磁性能进行表征,用扫描电子显微镜对颗粒形貌进行表征。从表征结果可知,由铁砂直接合成铁氧体镁,无需前期加工成磁铁矿矿物。加入四面体醋酸镁,在70℃的搅拌温度下,对样品进行了磁性能测试。x射线衍射图显示优值为0.82,磁滞曲线显示矫顽力为200 Oe,磁矩约为11 emu/gr。这种矿物具有不规则的颗粒大小,大小在0.5到100微米之间,这是由于磁性吸引促进了团聚。本研究建议对合成工艺进行优化,以提高铁氧体镁的质量。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Sintesis Magnesium Ferit Berbasis Pasir Besi dari Sarmi menggunakan Metode Kopresipitasi
In this study, magnesium ferrite was sinthesized from natural iron sand using co-precipitation method. Iron sand material was taken from the north coast of Sarmi Regency, Papua Province. The purpose of this study was to find out whether magnesium ferrite could be synthesized from iron sand directly without preliminary processes into magnetite minerals. Co-precipitation method was applied with a variant of stirring temperature of 30, 50 and 70°C. The crystal structures was characterized using an x-ray diffractometer, while the magnetic properties was characterized using a vibrating sample magnetometer and the morphology of the particle was characterized using a scanning electron microscpe. From the results of characterization, it is known that magnesium ferrite successfully synthesized from iron sand directly without preliminary processes into magnetite minerals. Magnetic properties were obtained from the sample with added of magnesium acetate tetrahedral and stirred at a temperature of 70°C. The x-ray diffracttion pattern showed figure of merit of 0.82, while the magnetic hysterisis curve shows coercivity of 200 Oe and magnetic moment about 11 emu/gr. The mineral has irregular particle sizes that range from 0.5 to 100 microns in size, due to magnetic attraction which promotes agglomeration. This researcher recommends optimization of the synthesis process so that the quality of the magnesium ferrite can be improve.
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