新型环β-二酮的高效超声合成、表征及抗菌筛选

N. Korde, S. Gaikwad, B. Khade, A. Rajbhoj, B. Ambedkar
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引用次数: 4

摘要

以2-乙酰苯甲酸乙酯为原料,采用贝克-文卡特拉曼转化法和超声辐照法合成了羟基苯基-3-丙烷,1,3-二酮4(LA-LF)。根据元素和光谱分析(IR, 1h NMR, 13c NMR, UV/Vis, Mass)确定了合成化合物的结构。对合成的化合物进行了抗菌和抗真菌活性评价。利用超声波照射,简单的反应条件,分离和纯化使得这种操作从经济和环境的角度来看非常有趣。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Efficient Ultrasound Synthesis, Characterizations and Antimicrobial Screening of Novel Cyclic β-Diketones
Hydroxyphenyl)-3-propane,1,3-diones 4(LA-LF) have been synthesized by a simple and convenient method employing Baker-Venkatraman transformation on corresponding 2- acetylphenyl benzoate by conventional as well as ultrasound irradiation method. The structure of synthesized compounds has been assigned on the basis of elemental and spectral analysis (IR, 1 H NMR, 13 C NMR, UV/Vis, Mass). The synthesized compounds were evaluated for antibacterial and antifungal activities. Utilization of ultrasound irradiation, simple reaction conditions, isolation and purification makes this manipulation very interesting from an economic and environmental perspective.
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