利用生物废弃物资源合成SiO2-CaO-Na2O玻璃及其体外生物活性研究

P. Srinath, P. A. Azeem, K. V. Reddy, S. R. Kumar
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引用次数: 2

摘要

本文介绍了利用生物废弃物制备二氧化硅- cao - na2o生物玻璃及其体外生物活性。稻壳灰和蛋壳生物废弃物分别作为提取二氧化硅和氧化钙的资源。玻璃样品采用标准熔融淬火技术制备。通过体外模拟体液(SBF)研究评估其生物活性。采用XRD、FTIR和SEM-EDS表征羟基磷灰石的成核和生长。XRD证实了羟基磷灰石的物相,与JCPDS标准数据吻合良好。FTIR光谱显示了明显的硅酸盐拉伸、弯曲振动模式和磷酸盐吸收带。表面形貌已观察到使用扫描电镜图像产生球形的羟基磷灰石形成。通过能谱分析,确定了磷灰石中的钙、磷等化学成分。这些结果完美地证明了RHA和蛋壳是生产生物玻璃的潜在有益来源。本文介绍了利用生物废弃物制备二氧化硅- cao - na2o生物玻璃及其体外生物活性。稻壳灰和蛋壳生物废弃物分别作为提取二氧化硅和氧化钙的资源。玻璃样品采用标准熔融淬火技术制备。通过体外模拟体液(SBF)研究评估其生物活性。采用XRD、FTIR和SEM-EDS表征羟基磷灰石的成核和生长。XRD证实了羟基磷灰石的物相,与JCPDS标准数据吻合良好。FTIR光谱显示了明显的硅酸盐拉伸、弯曲振动模式和磷酸盐吸收带。表面形貌已观察到使用扫描电镜图像产生球形的羟基磷灰石形成。通过能谱分析,确定了磷灰石中的钙、磷等化学成分。这些结果完美地证明了RHA和蛋壳是潜在的有益的生产生物蛋白的来源。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and in vitro bioactivity of SiO2-CaO-Na2O glass using bio-waste resources
The present paper describes the synthesis and in vitro bioactivity of SiO2-CaO-Na2O bio-glass using bio-waste. Rice husk ash (RHA) and eggshells bio-waste have been used as resources for extracting the silicon dioxide and calcium oxide respectively. Glass samples were obtained by standard melt-quenching technique. The bioactivity was assessed using in vitro studies in simulated body fluid (SBF). The nucleation and growth of hydroxyapatite were confirmed using XRD, FTIR and SEM-EDS characterizations. XRD have confirmed the phase of hydroxyapatite, well matched with its standard JCPDS data. FTIR spectra reveal the apparent silicate stretching, bending vibration modes and phosphate absorption bands. Surface morphology has been observed using SEM images resulting globular shape of hydroxyapatite formed. And, the chemical constituents of apatite such as Ca and P have been confirmed by EDS spectra. These results perfectly established that, RHA and eggshells are potentially beneficial sources for producing bio-glasses.The present paper describes the synthesis and in vitro bioactivity of SiO2-CaO-Na2O bio-glass using bio-waste. Rice husk ash (RHA) and eggshells bio-waste have been used as resources for extracting the silicon dioxide and calcium oxide respectively. Glass samples were obtained by standard melt-quenching technique. The bioactivity was assessed using in vitro studies in simulated body fluid (SBF). The nucleation and growth of hydroxyapatite were confirmed using XRD, FTIR and SEM-EDS characterizations. XRD have confirmed the phase of hydroxyapatite, well matched with its standard JCPDS data. FTIR spectra reveal the apparent silicate stretching, bending vibration modes and phosphate absorption bands. Surface morphology has been observed using SEM images resulting globular shape of hydroxyapatite formed. And, the chemical constituents of apatite such as Ca and P have been confirmed by EDS spectra. These results perfectly established that, RHA and eggshells are potentially beneficial sources for producing bio-g...
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