M. E. Glaoui, R. Kefi, E. Jeanneaub, F. Lefebvrec, C. Nasr
{"title":"三水合四氯酸双(5-氯-2,4-二甲氧基苯胺)的晶体结构","authors":"M. E. Glaoui, R. Kefi, E. Jeanneaub, F. Lefebvrec, C. Nasr","doi":"10.2174/1874846500902010001","DOIUrl":null,"url":null,"abstract":"The new inorganic-organic hybrid complex of Zn(II) with 5-Chloro-2,4-dimethoxyaniline, (5-Cl-2,4- (OCH3)2C6H2NH3)2ZnCl4.3H2O, has been prepared and characterized by X-ray crystallography. The complex crystallizes in the triclinic space group P1 with a = 7.4614 (2), b = 9.8734 (2), c = 18.5678 (4) A, = 102.3578 (14), = 91.0686 (15), = 91.2373 (12)°, V = 1335.49 (5) A 3 , Z = 2. Crystal structure has been determined and refined to R = 0.035 and Rw = 0.036 using 5107 independent reflections. In the atomic arrangement of the title compound, ZnCl4 2- inorganic entities, water molecule and -NH3 + groups have a layered organization around the planes z = 1/4 and z = 3/4. The crystal structure","PeriodicalId":23072,"journal":{"name":"The Open Crystallography Journal","volume":"23 1","pages":"1-5"},"PeriodicalIF":0.0000,"publicationDate":"2009-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"Crystal Structure of Bis(5-Chloro-2,4-Dimethoxyanilinium) Tetrachlorozincate Trihydrate\",\"authors\":\"M. E. Glaoui, R. Kefi, E. Jeanneaub, F. Lefebvrec, C. Nasr\",\"doi\":\"10.2174/1874846500902010001\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The new inorganic-organic hybrid complex of Zn(II) with 5-Chloro-2,4-dimethoxyaniline, (5-Cl-2,4- (OCH3)2C6H2NH3)2ZnCl4.3H2O, has been prepared and characterized by X-ray crystallography. The complex crystallizes in the triclinic space group P1 with a = 7.4614 (2), b = 9.8734 (2), c = 18.5678 (4) A, = 102.3578 (14), = 91.0686 (15), = 91.2373 (12)°, V = 1335.49 (5) A 3 , Z = 2. Crystal structure has been determined and refined to R = 0.035 and Rw = 0.036 using 5107 independent reflections. In the atomic arrangement of the title compound, ZnCl4 2- inorganic entities, water molecule and -NH3 + groups have a layered organization around the planes z = 1/4 and z = 3/4. The crystal structure\",\"PeriodicalId\":23072,\"journal\":{\"name\":\"The Open Crystallography Journal\",\"volume\":\"23 1\",\"pages\":\"1-5\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2009-01-21\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"The Open Crystallography Journal\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2174/1874846500902010001\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"The Open Crystallography Journal","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2174/1874846500902010001","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Crystal Structure of Bis(5-Chloro-2,4-Dimethoxyanilinium) Tetrachlorozincate Trihydrate
The new inorganic-organic hybrid complex of Zn(II) with 5-Chloro-2,4-dimethoxyaniline, (5-Cl-2,4- (OCH3)2C6H2NH3)2ZnCl4.3H2O, has been prepared and characterized by X-ray crystallography. The complex crystallizes in the triclinic space group P1 with a = 7.4614 (2), b = 9.8734 (2), c = 18.5678 (4) A, = 102.3578 (14), = 91.0686 (15), = 91.2373 (12)°, V = 1335.49 (5) A 3 , Z = 2. Crystal structure has been determined and refined to R = 0.035 and Rw = 0.036 using 5107 independent reflections. In the atomic arrangement of the title compound, ZnCl4 2- inorganic entities, water molecule and -NH3 + groups have a layered organization around the planes z = 1/4 and z = 3/4. The crystal structure
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