{"title":"微波辐照高效合成新型6-硝基苯并噻唑","authors":"Yves Njoya, A. Gellis, M. Crozet, P. Vanelle","doi":"10.1080/0278611031000104970","DOIUrl":null,"url":null,"abstract":"2-Chloromethyl-6-nitrobenzothiazole 2 is obtained by cyclocondensation of 2-aminobenzenethiol and chloroacetic acid. This product allows the synthesis of 2-alkyl-6-nitrobenzothiazoles 5, 17-24 under microwave activation via an electron transfer reaction by successive C-alkylation of nitronate anions 3, 6-13 and nitrous acid elimination.","PeriodicalId":22122,"journal":{"name":"Sulfur Letters","volume":"28 1","pages":"67 - 75"},"PeriodicalIF":0.0000,"publicationDate":"2003-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"17","resultStr":"{\"title\":\"Efficient synthesis of new 6-nitrobenzothiazoles using microwave irradiation\",\"authors\":\"Yves Njoya, A. Gellis, M. Crozet, P. Vanelle\",\"doi\":\"10.1080/0278611031000104970\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"2-Chloromethyl-6-nitrobenzothiazole 2 is obtained by cyclocondensation of 2-aminobenzenethiol and chloroacetic acid. This product allows the synthesis of 2-alkyl-6-nitrobenzothiazoles 5, 17-24 under microwave activation via an electron transfer reaction by successive C-alkylation of nitronate anions 3, 6-13 and nitrous acid elimination.\",\"PeriodicalId\":22122,\"journal\":{\"name\":\"Sulfur Letters\",\"volume\":\"28 1\",\"pages\":\"67 - 75\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2003-04-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"17\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Sulfur Letters\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1080/0278611031000104970\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Sulfur Letters","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/0278611031000104970","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Efficient synthesis of new 6-nitrobenzothiazoles using microwave irradiation
2-Chloromethyl-6-nitrobenzothiazole 2 is obtained by cyclocondensation of 2-aminobenzenethiol and chloroacetic acid. This product allows the synthesis of 2-alkyl-6-nitrobenzothiazoles 5, 17-24 under microwave activation via an electron transfer reaction by successive C-alkylation of nitronate anions 3, 6-13 and nitrous acid elimination.
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