溶液燃烧法混合燃料法制备ZnO纳米颗粒的结构与发光性能

T. K. Pathak, H. Swart
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引用次数: 1

摘要

氧化锌已用于许多应用,例如光电器件,陶瓷,催化剂,颜料,压敏电阻和许多其他重要应用。在本研究中,采用溶液燃烧的混合燃料方法合成了ZnO纳米颗粒。尿素、甘氨酸和柠檬酸的混合物在室温下与硝酸锌作为燃料混合,导致自燃,从而产生纳米氧化锌粉末。采用x射线衍射仪(XRD)对合成的ZnO纳米粉体的晶体结构和粒径进行了测定,结果表明合成的ZnO纳米粉体具有纯纤锌矿结构,晶粒尺寸为26 ~ 40 nm。利用红外光谱和紫外-可见吸收光谱对纳米材料进行了光学研究。在325 nm激发下,在360 ~ 800 nm可见光区进行了发光研究。这些纳米材料可用于固态照明器件。燃料含量对燃烧法合成的氧化锌纳米晶粉末的发光性能和抗菌性能的影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Structural and Luminescence Properties of ZnO Nanoparticles Synthesized by Mixture of Fuel Approach in Solution Combustion Method
Zinc oxide has been used for many applications, for example optoelectronic devices, ceramics, catalysts, pigments, varistors and many other important applications. In this study, ZnO nanoparticles were synthesized by mixture of fuel approach in solution combustion method. Mixtures of urea, glycine and citric acid were mixed at room temperature with Zinc nitrates as fuels resulting in spontane-ous ignition resulting in production of ZnO nanopowder. The crystal structure and size of the synthesized powder were determined by X-ray diffractometer (XRD), which revealed that the synthesized ZnO nanopowder has the pure wurtzite structure having crystallite size 26–40 nm. Optical studies of nanomaterial were examined by FTIR and UV-Visible absorption spectrum. The luminescence studies also investigated in the visible region 360–800 nm with excitation 325 nm laser. These nanomaterials may be used in solid-state lightening devices. of fuel content on luminescence and antibacterial properties of zinc oxide nanocrystalline powders synthesized by the combustion method.”
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