S. Cherrouf, Y. Salhi, Amina El Echhab, Hassan El Grini, Jihane Tellal, M. Cherkaoui, B. Lakhrissi
{"title":"添加和不添加葡萄糖基添加剂锡镀层的电化学研究与表征","authors":"S. Cherrouf, Y. Salhi, Amina El Echhab, Hassan El Grini, Jihane Tellal, M. Cherkaoui, B. Lakhrissi","doi":"10.13171/mjc02110281589salhi","DOIUrl":null,"url":null,"abstract":"The tin coating was elaborated electrolytically on an ordinary steel substrate in SnSO4 based electrolyte in acid medium with additive (bis-glycobenzimidazolone) at ambient temperature. The pH is maintained at 1.2±0.2 Bis-glycobenzimidazolone influence on the electrochemical properties of the tin coating was investigated using stationary polarization, chronopotentiometry, and cyclic voltammetry techniques. These studies show an apparent decrease in cathodic peak current and a drop in potential. The deposition rate also decreases as the concentration of the additive increases. SEM (Scanning Electron Microscopy) observation and XRD (X-ray Diffraction) analysis showed that the coating consists of good surface quality of the deposit elaborated by the addition of an optimal concentration of bis-glycobenzimidazolone (10-3M) in the electrolyte, which constitutes the continuation of a preliminary study.","PeriodicalId":18513,"journal":{"name":"Mediterranean Journal of Chemistry","volume":"68 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-10-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Electrochemical study and characterization of tin coatings with and without glucose-based additive\",\"authors\":\"S. Cherrouf, Y. Salhi, Amina El Echhab, Hassan El Grini, Jihane Tellal, M. Cherkaoui, B. Lakhrissi\",\"doi\":\"10.13171/mjc02110281589salhi\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The tin coating was elaborated electrolytically on an ordinary steel substrate in SnSO4 based electrolyte in acid medium with additive (bis-glycobenzimidazolone) at ambient temperature. The pH is maintained at 1.2±0.2 Bis-glycobenzimidazolone influence on the electrochemical properties of the tin coating was investigated using stationary polarization, chronopotentiometry, and cyclic voltammetry techniques. These studies show an apparent decrease in cathodic peak current and a drop in potential. The deposition rate also decreases as the concentration of the additive increases. SEM (Scanning Electron Microscopy) observation and XRD (X-ray Diffraction) analysis showed that the coating consists of good surface quality of the deposit elaborated by the addition of an optimal concentration of bis-glycobenzimidazolone (10-3M) in the electrolyte, which constitutes the continuation of a preliminary study.\",\"PeriodicalId\":18513,\"journal\":{\"name\":\"Mediterranean Journal of Chemistry\",\"volume\":\"68 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-10-28\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Mediterranean Journal of Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.13171/mjc02110281589salhi\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Mediterranean Journal of Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.13171/mjc02110281589salhi","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Electrochemical study and characterization of tin coatings with and without glucose-based additive
The tin coating was elaborated electrolytically on an ordinary steel substrate in SnSO4 based electrolyte in acid medium with additive (bis-glycobenzimidazolone) at ambient temperature. The pH is maintained at 1.2±0.2 Bis-glycobenzimidazolone influence on the electrochemical properties of the tin coating was investigated using stationary polarization, chronopotentiometry, and cyclic voltammetry techniques. These studies show an apparent decrease in cathodic peak current and a drop in potential. The deposition rate also decreases as the concentration of the additive increases. SEM (Scanning Electron Microscopy) observation and XRD (X-ray Diffraction) analysis showed that the coating consists of good surface quality of the deposit elaborated by the addition of an optimal concentration of bis-glycobenzimidazolone (10-3M) in the electrolyte, which constitutes the continuation of a preliminary study.