以蛋白为模板的微波辐射合成ZnO纳米结构

T. Prakash, R. Jayaprakash, G. Neri, Sanjay Kumar
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引用次数: 21

摘要

采用微波辐照法制备了氧化锌纳米结构。利用x射线衍射(XRD)、傅里叶红外光谱(FT-IR)、热重分析(TG-DTA)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)等技术研究了蛋白作为模板对ZnO尺寸和形貌的影响。在没有蛋白的情况下,得到了锌(OH)2和氧化锌的非均相混合物。在蛋白存在的情况下,获得了由棒状和须状纳米颗粒嵌入片状基质中的纯ZnO纳米结构。并比较了合成样品的光学和光致发光性能。研究结果表明,微波辅助法制备ZnO纳米结构是一种很有前途的低温、廉价、快速制备ZnO纳米结构的方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of ZnO Nanostructures by Microwave Irradiation Using Albumen as a Template
ZnO nanostructures have been successfully prepared by a microwave irradiation method. The role of albumen as a template in addressing the size and morphology of ZnO has been investigated by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TG-DTA), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. A heterogeneous mixture of Zn(OH)2 and ZnO was obtained in absence of albumen. Pure ZnO nanostructures, consisting of rod- and whisker-like nanoparticles embedded in a sheet matrix, were obtained in the presence of albumen. Optical and photoluminescence (PL) properties of the synthesized samples were also compared. Results obtained indicate that the microwave-assisted method is a promising low temperature, cheap, and fast method for the production of ZnO nanostructures.
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