微波等离子体原子发射光谱法测定含碲有机化合物中的碲

Lastovka Av, V. P. Fadeeva, M. A. Bazhenov, V. Tikhova
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引用次数: 1

摘要

提出了用Agilent 4100微波等离子体原子发射光谱仪测定含碲有机化合物(TOC)中碲的方法。样品分解方法之一-氧烧瓶燃烧或在加热块酸分解-可以应用。对碲含量在20 ~ 58%的碲二唑衍生物和其他TOC进行了分析。TOC中存在的氮、硫、钾、硒等元素并不妨碍碲的测定。分析的相对误差为1-5%。用安捷伦4100能谱仪对碲含量在20 ~ 58%之间的碲二唑衍生物及其它含碲有机化合物进行了分析
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Determination of Tellurium in Tellurium-Containing Organic Compounds by Microwave Plasma-Atomic Emission Spectrometry
A method for determining tellurium in tellurium-containing organic compounds (TOC) by a microwave plasmaatomic emission spectrometer Agilent 4100 has been suggested. One of the sample decomposition methods - the oxygen flask combustion or the acid decomposition in a heating block-can be applied. Telluradiazole derivatives and some other TOC with 20 to 58% tellurium content have been analyzed. Elements such as nitrogen, sulfur, potassium, selenium present in the TOC do not prevent from determining tellurium. The relative error of the analysis is 1-5%. Telluradiazole derivatives and some other tellurium-containing organic compounds with 20 to 58% tellurium content have been analysed by MP-AES spectrometer Agilent 4100
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