苊。第二部分。3,4-二氨基萘-1,8-二羧酸酐(3,4-二氨基萘酸酐)及其衍生物的制备

Journal of The Chemical Society C: Organic Pub Date : 1971-01-01 DOI:10.1039/J39710003891

L. A. Jones, H. K. Kim, R. Watson

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引用次数: 1

摘要

报道了先前未知的3,4-二氨基萘-1,8-二羧酸酐(7)的合成。在二烷基酯(16)和(17)的替代合成路线中发现了对结构指派的支持。所有的新化合物都是通过元素分析、红外光谱和核磁共振光谱来表征的。

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Acenaphthene. Part II. The preparation of 3,4-diaminonaphthalene-1,8-dicarboxylic anhydride (3,4-diaminonaphthalic anhydride) and derivatives

The synthesis of the previously unknown 3,4-diaminonaphthalene-1,8-dicarboxylic anhydride (7) is reported. Support for the structural assignment is found in an alternate synthetic route to the dialkyl esters (16) and (17). All new compounds are characterized by elemental analysis and i.r. and n.m.r. spectroscopy.

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Journal of The Chemical Society C: Organic

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