热离子真空电弧(TVA)技术沉积纳米结构Ti-C薄膜

V. Ciupină, R. Vlǎdoiu,  C. P. Lungu, C. Porosnicu, G. Prodan, E. Vasile, A.   MANDES, V. Dinca, A. Velea, V. Nicolescu
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引用次数: 0

摘要

采用热离子真空电弧(TVA)技术,在1 × 10-6Torr的高压下,在不同数量的Ti/C组合下制备了不同构型的纳米钛碳纳米薄膜。在硅衬底上沉积了约40nm的碳基层和7个40nm的Ti和C交替层。另一方面,为了获得变厚度、C层和Ti层中不同百分比的C-Ti多层结构,首先在Si衬底上沉积20nm厚的C层,然后沉积7层厚度达40nm的Ti-C层。通过改变C和Ti等离子体源的放电参数,实现不同厚度的连续分层。通过在室温到300℃之间改变衬底温度,另一方面偏置电压高达-700V,获得不同批次的样品。通过卢瑟福后向散射光谱(RBS)、拉曼光谱(Raman Spectroscopy)、透射电子显微镜(TEM)、掠入射x射线衍射(GIXRD)对膜的表面形貌和微观结构进行了表征。摩擦学和电学测量也被提出。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
NANOSTRUCTURED Ti-C THIN FILMS DEPOSITED BY THERMIONIC VACUUM ARC (TVA) TECHNOLOGY
Nanostructured titanium-carbon nanostructured thin films were prepared using the Thermionic Vacuum Arc (TVA) technology in different configurations under a varied number of Ti/C combinations at high base pressure of 1 x 10-6Torr with and without graded compositions. The layers consisting of about lOOnm Carbon base layer and seven 40nm alternatively Ti and C layers were deposited on Silicon substrates. On the other hand, in order to obtain C-Ti multilayer structures with variable thickness and different percentages in C and Ti oflayers, a 20nm thick C layer was first deposed on Si substrate and then seven Ti-C layers, each ofthese having thickness of up to 40nm were deposed. To perform the successively layers with various thickness were changed the discharge parameters for C and Ti plasma sources to obtain the desirable thickness. By changing ofsubstrate temperature between room temperature and 300°C and on the other hand the bias voltage up to -700V, different batches of samples were obtained for this study. The films were characterized by surface morphology, and microstructure, through Rutherford Backscattering Spectrometry (RBS), Raman Spectroscopy, Transmission Electron Microscopy (TEM), Grazing Incidence X-ray diffraction (GIXRD). Tribological and electrical measurements are also presented.
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