{"title":"沉淀法制备铌酸铅钪陶瓷的表征","authors":"Chude Feng, W. Schulze","doi":"10.1111/J.1551-2916.1988.TB00259.X","DOIUrl":null,"url":null,"abstract":"The synthesized monosized PSN complex precursor powder was produced using the methods of the controlled hydrolysis of Nb(OC{sub 2}H{sub 5}){sub 5} and the growth of scandium and lead carbonates on the as-hydrolyzed Nb{sub 2}O{sub 5} particle surface. Calcining the carbonates to oxides and sintering at different temperatures with various cooling rates produced dense ceramics. The relation between dielectric relaxation character and structural ordering of the sintered PSN ferroelectric ceramics was investigated.","PeriodicalId":7260,"journal":{"name":"Advanced Ceramic Materials","volume":"99 1","pages":"473-477"},"PeriodicalIF":0.0000,"publicationDate":"1988-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"4","resultStr":"{\"title\":\"Characterization of lead scandium niobate ceramics prepared by precipitation method\",\"authors\":\"Chude Feng, W. Schulze\",\"doi\":\"10.1111/J.1551-2916.1988.TB00259.X\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The synthesized monosized PSN complex precursor powder was produced using the methods of the controlled hydrolysis of Nb(OC{sub 2}H{sub 5}){sub 5} and the growth of scandium and lead carbonates on the as-hydrolyzed Nb{sub 2}O{sub 5} particle surface. Calcining the carbonates to oxides and sintering at different temperatures with various cooling rates produced dense ceramics. The relation between dielectric relaxation character and structural ordering of the sintered PSN ferroelectric ceramics was investigated.\",\"PeriodicalId\":7260,\"journal\":{\"name\":\"Advanced Ceramic Materials\",\"volume\":\"99 1\",\"pages\":\"473-477\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1988-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"4\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Advanced Ceramic Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1111/J.1551-2916.1988.TB00259.X\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Advanced Ceramic Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1111/J.1551-2916.1988.TB00259.X","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Characterization of lead scandium niobate ceramics prepared by precipitation method
The synthesized monosized PSN complex precursor powder was produced using the methods of the controlled hydrolysis of Nb(OC{sub 2}H{sub 5}){sub 5} and the growth of scandium and lead carbonates on the as-hydrolyzed Nb{sub 2}O{sub 5} particle surface. Calcining the carbonates to oxides and sintering at different temperatures with various cooling rates produced dense ceramics. The relation between dielectric relaxation character and structural ordering of the sintered PSN ferroelectric ceramics was investigated.
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