高强度超声辅助浓缩咖啡油甲酯酯交换反应:响应面法优化

Krit Somnuk, Pichai Eawlex, Jarernporn Thawornprasert, G. Prateepchaikul
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引用次数: 1

摘要

利用高强度超声催化碱催化酯交换反应,加速了浓缩咖啡油(ECO)生产生物柴油的酯转化。采用响应面法(RSM),通过甲醇、氢氧化钾和超声反应时间三个参数对ECO生物柴油的酯转化率进行了优化。ECO经过超声波均质机(超声功率1000W,超声频率18khz)生产生物柴油。在甲醇用量为30.8 vol.%,氢氧化钾浓度为16.6 gKOH/L,超声反应时间为72秒的条件下,得到的甲酯最高收率为96.385 wt.%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
High Intensity Ultrasound Assisted Transesterification of Espresso Coffee Oil Methyl Ester: Optimization through Response Surface Methodology Approach
High intensity ultrasound was used to accelerate the ester conversion of biodiesel production from espresso coffee oil (ECO) with a base-catalyzed transesterification. The ester conversion from ECO biodiesel production was optimized through three parameters: methanol, potassium hydroxide, and ultrasonic reaction time with a response surface methodology (RSM). After ECO has gone through the ultrasonic homogenizer (1000W ultrasonic power, 18 kHz ultrasonic frequency) for the biodiesel production. The maximum methyl ester of 96.385 wt.% was achieved under an optimal condition: 30.8 vol.% methanol, 16.6 gKOH/L, and 72 sec ultrasonic reaction time.
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