Cu/Nb纳米复合线的FIM和三维原子探针分析

X Sauvage , L Thilly , F Lecouturier , A Guillet , D Blavette
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引用次数: 21

摘要

采用场离子显微镜(FIM)和三维原子探针对两种Cu/Nb纳米复合线进行了研究。这两种技术首次揭示了纳米复合线材截面的纳米级微观结构。FIM研究证实了Cu和Nb织构以及(111)Cu和(110)Nb平面之间的失向。还观察到低角度Nb/Nb晶界。得益于三维原子探针,部分铌纤维和几纳米宽的铜通道被三维绘制出来。Cu/Nb界面光滑归因于应力诱导扩散。观察到的垂直于导线轴线的剪切带归因于铜通道中移动位错的轨迹。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
FIM and 3D atom probe analysis of Cu/Nb nanocomposite wires

Two kinds of Cu/Nb nanocomposite wires were investigated using field ion microscopy (FIM) and 3D atom probe. These two techniques revealed for the first time the nanoscale microstructure of nanocomposite wire cross sections. FIM investigations confirmed the Cu and Nb texture and the disorientation between (111) Cu and (110) Nb planes. Low angle Nb/Nb grain boudaries were also observed. Thanks to 3D atom probe, parts of niobium fibres and copper channels a few nanometer width were mapped out in 3D. Smooth Cu/Nb interfaces were attributed to stress-induced diffusion. Shear bands, observed perpendicular to the wire axis, were attributed to tracks of moving dislocations in a copper channel.

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