溶胶-凝胶自燃烧法制备铁氧体镁的电导率

Sudhanshu Kumar, K. Sreenivas
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引用次数: 3

摘要

以dl -丙氨酸为燃料,采用溶胶-凝胶自燃烧法制备了铁酸镁(MgFe2O4)粉体。将得到的烧成粉末在600 ~ 1300℃的不同温度下退火4小时。在900℃的最佳温度下得到相纯粉末,无机MgFe2O4中残余碳、氮、氢含量较低。高电阻MgFe2O4陶瓷通过在1200°C烧结得到,并且发现从频率和温度相关的交流电导率分析显示出半导体行为。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Electrical conductivity of magnesium ferrite prepared by sol-gel auto combustion technique
Magnesium ferrite (MgFe2O4) powder has been synthesized by sol-gel auto combustion method using DL-alanine fuel. The obtained as-burnt powder was annealed at different temperatures in the range 600 to 1300 °C for 4 hrs. Phase pure powders are obtained at an optimum temperature of 900 °C, and the residual carbon, nitrogen and hydrogen content in the inorganic MgFe2O4 are found to be low. Highly resistive MgFe2O4 ceramics are obtained by sintering at 1200 °C, and are found to exhibit semiconducting behavior as analyzed from the frequency and temperature dependent ac conductivity.
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