{"title":"溶胶-凝胶自燃烧法制备铁氧体镁的电导率","authors":"Sudhanshu Kumar, K. Sreenivas","doi":"10.1063/1.5122341","DOIUrl":null,"url":null,"abstract":"Magnesium ferrite (MgFe2O4) powder has been synthesized by sol-gel auto combustion method using DL-alanine fuel. The obtained as-burnt powder was annealed at different temperatures in the range 600 to 1300 °C for 4 hrs. Phase pure powders are obtained at an optimum temperature of 900 °C, and the residual carbon, nitrogen and hydrogen content in the inorganic MgFe2O4 are found to be low. Highly resistive MgFe2O4 ceramics are obtained by sintering at 1200 °C, and are found to exhibit semiconducting behavior as analyzed from the frequency and temperature dependent ac conductivity.","PeriodicalId":7262,"journal":{"name":"ADVANCES IN BASIC SCIENCE (ICABS 2019)","volume":"86 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-08-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Electrical conductivity of magnesium ferrite prepared by sol-gel auto combustion technique\",\"authors\":\"Sudhanshu Kumar, K. Sreenivas\",\"doi\":\"10.1063/1.5122341\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Magnesium ferrite (MgFe2O4) powder has been synthesized by sol-gel auto combustion method using DL-alanine fuel. The obtained as-burnt powder was annealed at different temperatures in the range 600 to 1300 °C for 4 hrs. Phase pure powders are obtained at an optimum temperature of 900 °C, and the residual carbon, nitrogen and hydrogen content in the inorganic MgFe2O4 are found to be low. Highly resistive MgFe2O4 ceramics are obtained by sintering at 1200 °C, and are found to exhibit semiconducting behavior as analyzed from the frequency and temperature dependent ac conductivity.\",\"PeriodicalId\":7262,\"journal\":{\"name\":\"ADVANCES IN BASIC SCIENCE (ICABS 2019)\",\"volume\":\"86 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-08-29\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"ADVANCES IN BASIC SCIENCE (ICABS 2019)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1063/1.5122341\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"ADVANCES IN BASIC SCIENCE (ICABS 2019)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/1.5122341","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Electrical conductivity of magnesium ferrite prepared by sol-gel auto combustion technique
Magnesium ferrite (MgFe2O4) powder has been synthesized by sol-gel auto combustion method using DL-alanine fuel. The obtained as-burnt powder was annealed at different temperatures in the range 600 to 1300 °C for 4 hrs. Phase pure powders are obtained at an optimum temperature of 900 °C, and the residual carbon, nitrogen and hydrogen content in the inorganic MgFe2O4 are found to be low. Highly resistive MgFe2O4 ceramics are obtained by sintering at 1200 °C, and are found to exhibit semiconducting behavior as analyzed from the frequency and temperature dependent ac conductivity.