{"title":"2,7-双(苯基磺酰)-2,7-二甲基-4-炔-3,6-二酮的晶体结构","authors":"K. Banert, I. Scharf, T. Rüffer, H. Lang","doi":"10.2116/ANALSCIX.24.X213","DOIUrl":null,"url":null,"abstract":"The title compound crystallizes in the triclinic space group P1 with a = 9.55(3), b = 10.61(4), c = 10.76(4)A, α = 101.25(6), β = 95.96(6), γ = 94.64(6)°, V = 1058(7)A3, and Z = 2. An X-ray structure analysis of this compound proves a surprising constitution of a product, which is formed in a new type of rearrangement reaction.","PeriodicalId":7796,"journal":{"name":"Analytical Sciences: X-ray Structure Analysis Online","volume":"121 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2008-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Crystal Structure of 2,7-Bis(phenylsulfanyl)-2,7-dimethyloct-4-yne-3,6-dione\",\"authors\":\"K. Banert, I. Scharf, T. Rüffer, H. Lang\",\"doi\":\"10.2116/ANALSCIX.24.X213\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The title compound crystallizes in the triclinic space group P1 with a = 9.55(3), b = 10.61(4), c = 10.76(4)A, α = 101.25(6), β = 95.96(6), γ = 94.64(6)°, V = 1058(7)A3, and Z = 2. An X-ray structure analysis of this compound proves a surprising constitution of a product, which is formed in a new type of rearrangement reaction.\",\"PeriodicalId\":7796,\"journal\":{\"name\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"volume\":\"121 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Analytical Sciences: X-ray Structure Analysis Online\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.2116/ANALSCIX.24.X213\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Analytical Sciences: X-ray Structure Analysis Online","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.2116/ANALSCIX.24.X213","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
标题化合物在三斜空间群P1中结晶，a = 9.55(3)， b = 10.61(4)， c = 10.76(4) a， α = 101.25(6)， β = 95.96(6)， γ = 94.64(6)°，V = 1058(7)A3, Z = 2。该化合物的x射线结构分析证明了一种令人惊讶的产物结构，它是在一种新型重排反应中形成的。
Crystal Structure of 2,7-Bis(phenylsulfanyl)-2,7-dimethyloct-4-yne-3,6-dione
The title compound crystallizes in the triclinic space group P1 with a = 9.55(3), b = 10.61(4), c = 10.76(4)A, α = 101.25(6), β = 95.96(6), γ = 94.64(6)°, V = 1058(7)A3, and Z = 2. An X-ray structure analysis of this compound proves a surprising constitution of a product, which is formed in a new type of rearrangement reaction.
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