Mukhtar Ghozali, Gamaliel Tanaka, Muhammad Misbahussalam, Tifa Paramitha
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摘要

ZSM-5是一种合成沸石,其生产工艺复杂,受操作条件(如温度和时间)的影响。本研究采用水热法无模板合成ZSM-5。热压釜反应器用于水热工艺。研究热液温度为180oC,热液时间为24小时和48小时对ZSM-5特性的影响。所使用的原料是氧化硅和氢氧化铝作为二氧化硅和氧化铝的来源。用x射线衍射(XRD)对合成结果进行了表征。XRD结果表明,在水热时间为48 h时,ZSM-5材料在22.20的位置形成。热液作用48小时,样品的结晶度为51.3%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Pengaruh Waktu Hidrotermal terhadap Karakteristik Zeolite Socony Mobile-5 (ZSM-5) Tanpa Template Menggunakan Reaktor Autoclave
ZSM-5 is a synthetic zeolite which has a complex production process and is affected by operating conditions, such as temperature and time. In this study, synthesized ZSM-5 without template by hydrothermal method. An autoclave reactor was used for the hydrothermal process. The aim of this study was to investigate the effect of varied hydrothermal times of 24 and 48 hours with a hydrothermal temperature of 180oC on the characteristic of ZSM-5. The raw materials used were silica oxide and aluminum hydroxide as a source of silica and alumina. The synthesis results were characterized using X-Ray Diffraction (XRD). Based on XRD results, the best result was obtained in performed at 48 hours hydrothermal time indicating the formation of ZSM-5 material at the 22.2o position. The percentage crystallinity of the sample at the hydrothermal time of 48 hours was 51.3%.
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