微波介导椰水合成纳米金

P. J. Babu, R. Das, Anil Kumar, Utpal Bora
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引用次数: 28

摘要

摘要:本文报道了微波辐照法制备纳米金的方法。合成速度非常快,最佳合成时间为17 s。通过紫外可见光谱、透射电子显微镜(TEM)、高分辨率电子显微镜(HRTEM)和原子力显微镜(AFM)对所得颗粒进行了表征。合成的金纳米颗粒大部分为球形,平均直径为10.5±5 nm。通过x射线衍射(XRD)证实了金纳米颗粒的结晶性质。傅里叶变换红外(FTIR)分析表明,金纳米颗粒表面存在有机生物分子,这可能是金纳米颗粒稳定性的原因。对两种人类癌细胞系HeLa(人宫颈癌)和MCF-7(人乳腺癌)进行了细胞毒性测试,发现其无毒,从而证明了其生物相容性。该方法利用了一种廉价且容易获得的生物材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Microwave-Mediated Synthesis of Gold Nanoparticles Using Coconut Water
ABSTRACT We report the synthesis of gold nanoparticles using coconut water through microwave irradiation. Synthesis was found to be very rapid with an optimum time of 17 s. The particles obtained were characterized by UV-visible spectroscopy, transmission electron microscopy (TEM), high-resolution TEM (HRTEM), and atomic force microscopy (AFM). The synthesized gold nanoparticles were found to be mostly spherical with an average diameter of 10.5 ± 5 nm. The crystalline nature of gold nanoparticles was confirmed by X-ray diffraction (XRD) patterns. Fourier transform infrared (FTIR) analysis suggested the presence of organic biomolecules on the surface of the gold nanoprticles, which may be responsible for the stability of the particles. Cytotoxicity of the gold nanoparticles was tested on two human cancer cell lines, HeLa (human cervical cancer) and MCF-7 (human breast cancer), and found to be nontoxic, which thus proved their biocompatibility. The method exploits a cheap and easily available biomaterial th...
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