A. A. Maslov, A. Nazarov, A. Nikolaev, E. Vardanyan, K. Ramazanov
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引用次数: 0
摘要
本文介绍了用x射线衍射仪和同步辐射源对Ti - Al - C体系涂层进行相组成研究的结果。在乙炔和氩气的混合介质中,采用双单组分钛和铝阴极阴极电弧沉积的方法,在钼和钛样品上沉积了一层基于Ti - Al - C体系的涂层。相组成研究结果表明,Ti2AlC和Ti2C相的形成与热处理方式有关。采用同步辐射技术,研究了样品在真空中加热至1500℃时涂层的相稳定性。结果表明,沉积后的涂层具有非晶态结构,真空退火后结晶形成Ti2AlC、Ti2C相和Ti - Al金属间化合物。
Investigation of coatings based on the Ti – Al – C system using synchrotron radiation and X-ray diffraction
The paper presents results of the phase composition investigations of coatings based on the Ti – Al – C system using an X-ray diffractometer and a synchrotron radiation source. A coating based on the Ti – Al – C system was deposited on molybdenum and titanium samples by cathodic-arc deposition from two single-component titanium and aluminum cathodes in a mixture of acetylene and argon. The results of the study of the phase composition showed that the formation of the Ti2AlC and Ti2C phases depends on the heat treatment mode. Using synchrotron radiation, the phase stability of the coating was studied when the sample was heated to 1500 °C in vacuum. It has been established that the coating after deposition has an amorphous structure, which crystallizes after annealing in vacuum with the formation of Ti2AlC, Ti2C phases and Ti – Al intermetallic compounds.