碳酸锌纳米颗粒结合荧光素染料合成新型光致发光粉体的潜在指纹检测研究

K. Pattarith, R. Benchawattananon
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引用次数: 0

摘要

指纹识别是犯罪现场的一种基本方法,但与犯罪嫌疑人的联系是非常重要的。将荧光粉末应用于被动指纹认证中,可以提高指纹检测的性能。本研究以碳酸锌和荧光素染料为主要前驱体,以乙醇为溶剂,采用溶剂热法制备了新型指纹粉。还用各种诊断工具检查了合成荧光粉的试验特征。利用扫描电镜(SEM)对其微观结构进行检测,利用紫外-可见漫反射光谱(DRS)对其进行吸收,利用x射线衍射(XRD)和波长分别为254 nm和366 nm的紫外光对其符号特征进行检测。合成指纹荧光粉的测试是通过用潜在指纹在表面上滑动来完成的。为了研究影响指纹检测的最佳条件,一般有以下几种纹理类型,包括玻璃、金属、塑料和陶瓷,以及光滑、曲线和粗糙表面的外观。本文还研究了保存时间和温度对试验检测的指纹的影响。对于合成荧光粉,其检测可用于不同类型的各个表面,具有良好的表面外观。常温下保存期30天以上,90℃温度下保存期15天以上,还可用于检测重叠明显的指纹。本研究表明,合成荧光粉末具有非常优异的性能,具有很高的可能性作为物证在法医过程中用于被动指纹的检测。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Study on the Novel Photoluminescence Powder Synthesized from Zinc Carbonate Nanoparticles Associated with Fluorescein Dye for its Latent Fingerprint Detection
Fingerprint verification in crime scene is a basic method, but it is very important thing to be linked to the offender. Using fluorescent powder in passive fingerprint authentication will increase the performance of fingerprint detection for an identification. In this study, the new fingerprint powder has been synthesized by solvothermal method using zinc carbonate and fluorescein dye as main precursor using ethanol as a solvent. The synthetic fluorescent powder is also inspected for trial features with various diagnostic tools. As follows, detecting a micro texture with scanning electron microscope (SEM), absorption with UV-vis diffuse reflectance spectroscopy (DRS), examining the notation characteristics with X-ray diffraction (XRD) and UV light at wavelength 254 nm and 366 nm. Testing of the synthetic fingerprint fluorescent powder is done by swiping on the surface with a latent fingerprint. For studying optimum conditions affecting the fingerprint detection, there are general following types of textures including glass, metal, plastic and ceramics, and the appearance of smooth, curve and rough surfaces. It is also studies on the effects of duration and temperature of the retention affecting the fingerprints which have been inspected by the trial. For the synthetic fluorescent powder, its inspection can be used on each surface of different types with a good surface appearance. It has a long retention period of more than 30 days at room temperature and more than 15 days at a temperature of 90oC, and it can also be used to detect the fingerprints with a clear overlap. From this study, it is demonstrated that the synthetic fluorescent powder has a very excellent performance and has high possibility to be used to detect the passive fingerprints as an object witness in forensic processes.
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