以过热水或蒸汽为唯一洗脱剂的苯乙酮和间甲酚固相萃取和热解吸

Joanne R. Bone, Roger M. Smith
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引用次数: 9

摘要

蒸汽或过热水可用于在高达220°C的温度下有效地从聚合物吸附剂中洗脱中等极性和非极性化合物,而不会降解分析物。苯乙酮和间甲酚,作为模型化合物,从稀水溶液中,使用固相萃取(SPE)陷阱填充聚苯二乙烯基苯(PS-DVB)或聚二乙烯基苯-co- n -乙烯基吡咯烷酮。该技术成本低,使用方便,是一种环保的洗脱液。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Solid phase extraction and thermal desorption of acetophenone and m-cresol using superheated water or steam as the sole eluent
Steam or superheated water can be used to efficiently elute moderately polar and non-polar compounds from polymeric sorbents at temperatures up to 220 °C without degradation of the analyte. Acetophenone and m-cresol, as model compounds, have been concentrated from dilute aqueous solutions, using solid phase extraction (SPE) traps packed with polystyrene–divinylbenzene (PS–DVB) or poly(divinylbenzene-co-N-vinylpyrrolidone). The technique offers low cost, ease of use and an environmentally friendly eluent.
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