白砂糖制备活性炭的研究

Muhammad Muhammad, Mulyawan Mulyawan, Muntasir Raihan Rahman, S. Suryati
{"title":"白砂糖制备活性炭的研究","authors":"Muhammad Muhammad, Mulyawan Mulyawan, Muntasir Raihan Rahman, S. Suryati","doi":"10.52088/ijesty.v2i2.246","DOIUrl":null,"url":null,"abstract":"Activated carbon that potentially acts as an adsorbent was prepared from granulated sugar. The activated sugar was prepared through a dehydration process followed by a chemical activation process with a concentrated NaOH solution. To comprehend the properties of prepared ready carbon, characterization of the carbon was needed to be conducted. The conducted methods for prepared activated carbon were FTIR for detecting present functional groups attached to carbon, BET to identify the porous structure of synthesized carbon, SEM method as a morphological indicating method on synthesized carbon, and carbon thermal stability characteristic information from the TGA method. It was found that the prepared activated carbon contained various functional groups. The distinguished functional groups presented were carboxylic acid, free alcohol, NH2, and SO3. The readily activated carbon showed a rough surface to enhance the adsorption process on the synthesized carbon from the SEM characterization method. BET on the readily activated carbon revealed that the activated carbon exhibited type IV isotherm, consisting dominantly of mesopores and micropores as a minority. TGA characterization method showed that the thermal stability of carbon was significantly unstable in the range of 100℃ and around 200℃. It implies that the prepared activated carbon contained OH as one of its functional groups. With all the characterization methods conducted on the readily activated carbon from granulated sugar, it was found that the prepared carbon had the potential to be utilized as an adsorbent. Moreover, it is suggested that the granular sugar-based carbon should be investigated in the following future study in the wastewater treatment process.","PeriodicalId":14149,"journal":{"name":"International Journal of Engineering, Science and Information Technology","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2022-04-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Characterization of Activated Carbon from Granulated Sugar\",\"authors\":\"Muhammad Muhammad, Mulyawan Mulyawan, Muntasir Raihan Rahman, S. Suryati\",\"doi\":\"10.52088/ijesty.v2i2.246\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Activated carbon that potentially acts as an adsorbent was prepared from granulated sugar. The activated sugar was prepared through a dehydration process followed by a chemical activation process with a concentrated NaOH solution. To comprehend the properties of prepared ready carbon, characterization of the carbon was needed to be conducted. The conducted methods for prepared activated carbon were FTIR for detecting present functional groups attached to carbon, BET to identify the porous structure of synthesized carbon, SEM method as a morphological indicating method on synthesized carbon, and carbon thermal stability characteristic information from the TGA method. It was found that the prepared activated carbon contained various functional groups. The distinguished functional groups presented were carboxylic acid, free alcohol, NH2, and SO3. The readily activated carbon showed a rough surface to enhance the adsorption process on the synthesized carbon from the SEM characterization method. BET on the readily activated carbon revealed that the activated carbon exhibited type IV isotherm, consisting dominantly of mesopores and micropores as a minority. TGA characterization method showed that the thermal stability of carbon was significantly unstable in the range of 100℃ and around 200℃. It implies that the prepared activated carbon contained OH as one of its functional groups. With all the characterization methods conducted on the readily activated carbon from granulated sugar, it was found that the prepared carbon had the potential to be utilized as an adsorbent. Moreover, it is suggested that the granular sugar-based carbon should be investigated in the following future study in the wastewater treatment process.\",\"PeriodicalId\":14149,\"journal\":{\"name\":\"International Journal of Engineering, Science and Information Technology\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-04-26\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Engineering, Science and Information Technology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.52088/ijesty.v2i2.246\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Engineering, Science and Information Technology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.52088/ijesty.v2i2.246","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

以砂糖为原料制备了具有吸附剂作用的活性炭。通过脱水和浓NaOH溶液的化学活化法制备了活性糖。为了了解制备好的碳的性质,需要对碳进行表征。制备活性炭的主要方法有:FTIR法检测碳上的现有官能团,BET法鉴定合成碳的多孔结构,SEM法作为合成碳的形态指示方法,TGA法获得碳的热稳定性特征信息。结果表明,所制备的活性炭含有多种官能团。不同的官能团分别是羧酸、游离醇、NH2和SO3。SEM表征方法表明,易溶活性炭表面粗糙,增强了对合成碳的吸附过程。对易溶活性炭的BET结果表明,活性炭表现为IV型等温线,以中孔为主,微孔占少数。TGA表征方法表明,碳的热稳定性在100℃和200℃左右范围内明显不稳定。说明所制备的活性炭中含有OH作为其官能团之一。通过对砂糖制备的易感活性炭的各种表征方法,发现制备的活性炭具有作为吸附剂的潜力。此外,建议在后续的废水处理过程中对颗粒糖基碳进行研究。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Characterization of Activated Carbon from Granulated Sugar
Activated carbon that potentially acts as an adsorbent was prepared from granulated sugar. The activated sugar was prepared through a dehydration process followed by a chemical activation process with a concentrated NaOH solution. To comprehend the properties of prepared ready carbon, characterization of the carbon was needed to be conducted. The conducted methods for prepared activated carbon were FTIR for detecting present functional groups attached to carbon, BET to identify the porous structure of synthesized carbon, SEM method as a morphological indicating method on synthesized carbon, and carbon thermal stability characteristic information from the TGA method. It was found that the prepared activated carbon contained various functional groups. The distinguished functional groups presented were carboxylic acid, free alcohol, NH2, and SO3. The readily activated carbon showed a rough surface to enhance the adsorption process on the synthesized carbon from the SEM characterization method. BET on the readily activated carbon revealed that the activated carbon exhibited type IV isotherm, consisting dominantly of mesopores and micropores as a minority. TGA characterization method showed that the thermal stability of carbon was significantly unstable in the range of 100℃ and around 200℃. It implies that the prepared activated carbon contained OH as one of its functional groups. With all the characterization methods conducted on the readily activated carbon from granulated sugar, it was found that the prepared carbon had the potential to be utilized as an adsorbent. Moreover, it is suggested that the granular sugar-based carbon should be investigated in the following future study in the wastewater treatment process.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信