K. Aghapoor, H. R. Darabi, K. Tabar-Heydar, L. Nakhshab
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Synthesis of aliphatic thiomorpholides by willgerodt-kindler reaction under solvent-free conditions
The Willgerodt-Kindler reaction of aliphatic ketones and aldehydes with sulfur and morpholine under solvent-free conditions was performed in a domestic microwave oven. The method is simple, rapid and avoids prolonged heating with solvents.
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