葡萄糖酸钠的合成、表征及其对硅酸盐水泥性能的影响

Mahdee Muhammad Nafee, Umme Sarmeen Akhtar, Md. Sagirul Islam, M. E. Halim, M. G. Mostafa, Imdadul Haque
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引用次数: 0

摘要

研究了普通硅酸盐水泥(OPC)缓凝剂葡萄糖酸钠的合成、表征及其对水泥性能的影响。研究发现,葡萄糖酸钠延长了OPC的凝固时间,提高了和易性。以葡萄糖酸和氢氧化钠为原料,通过简单的化学反应合成了葡萄糖酸钠。利用红外傅立叶变换(FTIR)和核磁共振(1H-NMR)对合成产物进行了表征。结果表明,合成的葡萄糖酸钠在3205 cm2处有一个特征吸收峰。研究了凝固时间、抗压强度和孔隙率的变化。然而,较高的掺量延长了凝固时间,提高了和易性,降低了抗压强度,提高了孔隙率。该研究强调了平衡葡萄糖酸钠剂量与其他当地可用的外加剂的重要性,以获得所需的缓凝效果而不影响强度。需要进一步的研究来优化用量并探索对水泥性能的长期影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Sodium Gluconate and Its Effects on the Properties of Portland Cement
The research explores the synthesis and characterization of sodium gluconate as a retarding admixture for Ordinary Portland Cement (OPC) and its impact on cement properties. The study found that sodium gluconate prolonged OPC's setting time, enhancing workability. Sodium gluconate was synthesized through a simple chemical process involving the reaction of gluconic acid with sodium hydroxide. The synthesized product was characterized using Fourier Transform Infrared (FTIR) and 1H-NMR spectroscopy. The results showed that the synthesized sodium gluconate had a characteristic absorption peak at 3205 cm1.The variations were investigated for setting time, compressive strength, and porosity. However, higher dosages led to prolong the setting time, increased the workability, reduced compressive strength and improved porosity. The study emphasizes the importance of balancing sodium gluconate dosage with other locally available admixtures for desired retardation effects without compromising strength. Further research is needed to optimize dosage and explore long-term effects on cement properties.
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