Leila Masti, A. Bezaatpour, N. Bozari, Y. Azizian-Kalandaragh
{"title":"rGO/ZnFe2O4在可见光下光催化还原硝基芳香族化合物为相应的氨基芳香族化合物","authors":"Leila Masti, A. Bezaatpour, N. Bozari, Y. Azizian-Kalandaragh","doi":"10.22075/CHEM.2021.21751.1914","DOIUrl":null,"url":null,"abstract":"In this research work, the rGO/ZnFe2O4 photocatalyst was prepared by hydrothermal method and characterized and identified using X-ray powder diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), field emission scanning electron microscope (FE-SEM), Diffuse Reflectance Spectroscopy (DRS), vibrating-sample magnetometer (VSM), surface area analysis (BET) and Energy-dispersive X-ray spectroscopy (EDAX) techniques. The photocatalyst was used for the reduction of nitroaromatic compounds to their corresponding aromatic amines with hydrazine monohydrate. The catalyst showed the best activity in the reduction of 1,4-dinitrobenzen (%97 conversion in 40 min). The recyclability and reusability of the catalyst was evaluated for four times which showed no significant variation in the conversion of nitrobenzene photoreduction reaction.","PeriodicalId":7954,"journal":{"name":"Applied Chemistry","volume":"17 1","pages":"109-122"},"PeriodicalIF":0.0000,"publicationDate":"2021-09-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Photocatalytic reduction of nitro aromatic compounds to their corresponding amino aromatic compounds by rGO/ZnFe2O4 under visible light irradiation\",\"authors\":\"Leila Masti, A. Bezaatpour, N. Bozari, Y. Azizian-Kalandaragh\",\"doi\":\"10.22075/CHEM.2021.21751.1914\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this research work, the rGO/ZnFe2O4 photocatalyst was prepared by hydrothermal method and characterized and identified using X-ray powder diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), field emission scanning electron microscope (FE-SEM), Diffuse Reflectance Spectroscopy (DRS), vibrating-sample magnetometer (VSM), surface area analysis (BET) and Energy-dispersive X-ray spectroscopy (EDAX) techniques. The photocatalyst was used for the reduction of nitroaromatic compounds to their corresponding aromatic amines with hydrazine monohydrate. The catalyst showed the best activity in the reduction of 1,4-dinitrobenzen (%97 conversion in 40 min). The recyclability and reusability of the catalyst was evaluated for four times which showed no significant variation in the conversion of nitrobenzene photoreduction reaction.\",\"PeriodicalId\":7954,\"journal\":{\"name\":\"Applied Chemistry\",\"volume\":\"17 1\",\"pages\":\"109-122\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-09-23\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Applied Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.22075/CHEM.2021.21751.1914\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.22075/CHEM.2021.21751.1914","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Photocatalytic reduction of nitro aromatic compounds to their corresponding amino aromatic compounds by rGO/ZnFe2O4 under visible light irradiation
In this research work, the rGO/ZnFe2O4 photocatalyst was prepared by hydrothermal method and characterized and identified using X-ray powder diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), field emission scanning electron microscope (FE-SEM), Diffuse Reflectance Spectroscopy (DRS), vibrating-sample magnetometer (VSM), surface area analysis (BET) and Energy-dispersive X-ray spectroscopy (EDAX) techniques. The photocatalyst was used for the reduction of nitroaromatic compounds to their corresponding aromatic amines with hydrazine monohydrate. The catalyst showed the best activity in the reduction of 1,4-dinitrobenzen (%97 conversion in 40 min). The recyclability and reusability of the catalyst was evaluated for four times which showed no significant variation in the conversion of nitrobenzene photoreduction reaction.
求助内容：
应助结果提醒方式：
京公网安备 11010802042870号
