用x射线散射暗场层析成像技术表征注射成型短纤维增强聚合物的纤维结构

Christian Hannesschläger , Vincent Revol , Bernhard Plank , Dietmar Salaberger , Johann Kastner
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引用次数: 35

摘要

采用x射线散射暗场成像(SDFI)技术研究了短纤维增强聚合物(SFRPs)的玻璃纤维取向。纤维增强聚合物的纤维取向对注塑件的机械强度起决定性作用。本文采用体素尺寸为(43 μm)3的SDFI计算机断层扫描和体素尺寸为(6.5 μm)3的基于吸收的高分辨率x射线计算机断层扫描(XCT)对注塑件沿熔体流动和焊缝的四个不同位置进行了研究。将SDFI计算机断层扫描结果与纤维取向进行比较,研究SDFI信号对纤维取向的依赖关系。通过对高分辨率吸收XCT数据的评估,确定了纤维的确切取向。特别是,即使在体素尺寸为(43 μm)3的情况下,SDFI也可以表征焊缝和具有不同纤维取向的区域,并且可以检测到纤维取向特性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Fibre structure characterisation of injection moulded short fibre-reinforced polymers by X-ray scatter dark field tomography

X-ray scatter dark field imaging (SDFI) tomography was used to investigate the glass fibre orientation of short fibre-reinforced polymers (SFRPs). The fibre orientation of fibre-reinforced polymers is decisive for the mechanical strength of injection-moulded parts. For this paper four different positions, with volumes along the melt flow and with weld lines, of an injection-moulded part were investigated with SDFI computed tomography with a voxel size of (43 μm)3 and absorption-based high resolution X-ray computed tomography (XCT) with a voxel size of (6.5 μm)3. The results of the SDFI computed tomography are compared with the fibre orientation to investigate the dependence of the SDFI signal on fibre orientation. The exact fibre orientation was determined by evaluation of the high resolution absorption XCT data. In particular, it is shown that the weld line and areas with different fibre orientations can be characterised by SDFI even at a voxel size of (43 μm)3 and that fibre orientation properties can be detected.

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