水热法制备Cds纳米颗粒及其在不同生物用途上的贡献

H. Labiadh, A. Mezni, N. Loudhaief, Mouldizouaoui, M. Salem
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引用次数: 3

摘要

:在pH恒定的水介质中合成了硫化镉CdS纳米颗粒,用x射线衍射仪(XRD)和透射电镜(TEM)对纳米颗粒进行了表征。对硫化镉纳米颗粒进行抗菌筛选,并利用1,1-二苯基-2-癸酰肼(DPPH)、羟基自由基(OH)检测其抗氧化活性。过氧化氢(h2o2)清除活性,铁还原力(FRP)测定和铁离子螯合(FIC)方法。根据XRD数据,采用Debye-Scherrer公式估计晶体尺寸为12 nm。透射电镜(TEM)结果表明,CdS纳米晶体分布均匀,尺寸为12 nm。所得的CdS量子点具有抗氧化活性,特别是在氧化还原能力方面。结果表明,CdS纳米颗粒具有较高的抗氧化活性,其可在界面处与生命体发生反应。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of Cds Nanoparticle by the Hydrothermal Method and the Contribution in Different Biological Uses
: Cadmium sulfide CdS nanoparticles were synthesized in aqueous medium at pH constant, the obtained nanoparticles has been characterized by x-ray diffraction (XRD) and transmission electron microscopy (TEM). Cadmium sulfide nanoparticles were screened for their antibacterial and tested for antioxidant activity using 1,1-diphenyl-2-picrylhydrazyl (DPPH), hydroxyl radical (OH . ) and hydrogen peroxide (H 2 O 2 ) scavenging activity, ferric reducing power (FRP) assay and ferrous ion chelating (FIC) methods. The sizes of the crystallites were estimated to 12 nm using the Debye-Scherrer formula based on the XRD data. Transmission electron microscopy (TEM) results indicate that the CdS nanocrystals distribute uniformly and the size is 12 nm. The obtained CdS quantum dots present an antioxidant activity especially in oxido reduction power. It was found that CdS nanoparticles showed relatively higher antioxidant activities that this nanomaterial’ scan react at the interface with the life entities.
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