{"title":"秋葵植物提取物制备抗微生物Cr2O3纳米颗粒","authors":"Saja Q.Ali, Wisam J. Aziz, Raad S. Sabry","doi":"10.31257/2018/jkp/2021/130206","DOIUrl":null,"url":null,"abstract":"Cr2O3 NPs were synthesized using Okra extract with two methods; the simple chemical method and sol-gel method. XRD analysis showed that the crystal size of Cr2O3 in a simple chemical method was (16.15) nm and with sol-gel method were 16.6 nm, 16.14 nm and 16 nm using annealing temperature of 200, 400 and 600 °C respectively. FE-SEM analysis showed that the nanoparticles of Cr2O3 NPs when using a simple chemical and the sol-gel methods, with particle sizes of (83.74-132.1) nm, (18.92-27.68) nm, (24.19-39.08) nm, and (12.04-15.83) nm that corresponding to a simple chemical method at 200 °C, sol-gel method at 200, 400 and 600 °C respectively. UV-Vis demonstrated that the band gap value of Cr2O3 NPs was 2.9 eV with a simple chemical method, while in a sol-gel method was (3.15, 3.3, 3.5) eV at different temperatures. The study showed an effective antibacterial activity of Cr2O3 NPs such was (12-14) mm of Gram's negative bacteria and (15-18) mm for Gram's positive bacteria in simple chemical method at (200) °C. The higher antibacterial activity of three different temperatures of sol-gel method was (20) mm for Gram's negative bacteria and (23) mm for Gram's positive bacteria at 200°C.","PeriodicalId":16215,"journal":{"name":"Journal of Kufa - Physics","volume":"82 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-01-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Fabrication of Cr2O3 Nanoparticles Using Okra Plant Extract for Antimicrobial Activity\",\"authors\":\"Saja Q.Ali, Wisam J. Aziz, Raad S. Sabry\",\"doi\":\"10.31257/2018/jkp/2021/130206\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Cr2O3 NPs were synthesized using Okra extract with two methods; the simple chemical method and sol-gel method. XRD analysis showed that the crystal size of Cr2O3 in a simple chemical method was (16.15) nm and with sol-gel method were 16.6 nm, 16.14 nm and 16 nm using annealing temperature of 200, 400 and 600 °C respectively. FE-SEM analysis showed that the nanoparticles of Cr2O3 NPs when using a simple chemical and the sol-gel methods, with particle sizes of (83.74-132.1) nm, (18.92-27.68) nm, (24.19-39.08) nm, and (12.04-15.83) nm that corresponding to a simple chemical method at 200 °C, sol-gel method at 200, 400 and 600 °C respectively. UV-Vis demonstrated that the band gap value of Cr2O3 NPs was 2.9 eV with a simple chemical method, while in a sol-gel method was (3.15, 3.3, 3.5) eV at different temperatures. The study showed an effective antibacterial activity of Cr2O3 NPs such was (12-14) mm of Gram's negative bacteria and (15-18) mm for Gram's positive bacteria in simple chemical method at (200) °C. The higher antibacterial activity of three different temperatures of sol-gel method was (20) mm for Gram's negative bacteria and (23) mm for Gram's positive bacteria at 200°C.\",\"PeriodicalId\":16215,\"journal\":{\"name\":\"Journal of Kufa - Physics\",\"volume\":\"82 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-01-10\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Kufa - Physics\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.31257/2018/jkp/2021/130206\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Kufa - Physics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.31257/2018/jkp/2021/130206","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Fabrication of Cr2O3 Nanoparticles Using Okra Plant Extract for Antimicrobial Activity
Cr2O3 NPs were synthesized using Okra extract with two methods; the simple chemical method and sol-gel method. XRD analysis showed that the crystal size of Cr2O3 in a simple chemical method was (16.15) nm and with sol-gel method were 16.6 nm, 16.14 nm and 16 nm using annealing temperature of 200, 400 and 600 °C respectively. FE-SEM analysis showed that the nanoparticles of Cr2O3 NPs when using a simple chemical and the sol-gel methods, with particle sizes of (83.74-132.1) nm, (18.92-27.68) nm, (24.19-39.08) nm, and (12.04-15.83) nm that corresponding to a simple chemical method at 200 °C, sol-gel method at 200, 400 and 600 °C respectively. UV-Vis demonstrated that the band gap value of Cr2O3 NPs was 2.9 eV with a simple chemical method, while in a sol-gel method was (3.15, 3.3, 3.5) eV at different temperatures. The study showed an effective antibacterial activity of Cr2O3 NPs such was (12-14) mm of Gram's negative bacteria and (15-18) mm for Gram's positive bacteria in simple chemical method at (200) °C. The higher antibacterial activity of three different temperatures of sol-gel method was (20) mm for Gram's negative bacteria and (23) mm for Gram's positive bacteria at 200°C.