抗菌用半ipn银纳米复合水凝胶的研制与表征

A. Chandra Babu, M. Prabhakar, A. Suresh Babu, B. Mallikarjuna, M. Subha, K. Chowdoji Rao
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引用次数: 24

摘要

采用自由基聚合技术制备了羧甲基纤维素钠/聚(丙烯酰胺-co-2-丙烯酰胺-2-甲基丙烷磺酸)半互穿聚合物网络(半ipn)水凝胶。在半ipn水凝胶中,用硼水钠在室温下还原硝酸银形成纳米银。紫外可见光谱、热重分析、x射线衍射、扫描电子显微镜和透射电子显微镜技术被用来表征水凝胶中银纳米颗粒的形成。扫描电镜(SEM)图像清晰地显示了银纳米粒子群的形成,粒径范围在10 ~ 20 nm之间。透射电镜结果也支持银纳米颗粒的大小。本文报道的半ipn银纳米复合水凝胶在抗菌活性的应用范围内可能是一种潜在的智能材料。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Development and Characterization of Semi-IPN Silver Nanocomposite Hydrogels for Antibacterial Applications
Sodium carboxymethyl cellulose/poly(acrylamide-co-2-acrylamido-2-methylpropane sulfonic acid) semi-interpenetrating polymer network (semi-IPN) hydrogels were prepared by using free radical polymerization technique. Silver nanoparticles were formed by reduction of silver nitrate in semi-IPN hydrogels with sodium borohydrate at room temperature. UV-visible spectroscopy, thermogravimetrical analysis, X-ray diffractometry, scanning electron microscopy, and transmission electron microscopy techniques were used to characterize the formation of silver nanoparticles in hydrogels. SEM images indicated clearly the formation of group of silver nanoparticles with size range of 10–20 nm. The sizes of silver nanoparticles were also supported by transmission electron microscopy results. The semi-IPN silver nanocomposite hydrogels reported here might be a potentially smart material in the range of applications of antibacterial activity.
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