微波烧结3D打印绿色体制备多孔可生物降解铁支架的实验研究

D. Mishra, P. M. Pandey
{"title":"微波烧结3D打印绿色体制备多孔可生物降解铁支架的实验研究","authors":"D. Mishra, P. M. Pandey","doi":"10.1115/msec2021-63402","DOIUrl":null,"url":null,"abstract":"\n Iron has appealing biodegradable properties that makes compatible for biodegradable implant tools applications. Although, the slow corrosion rate of Fe made obsolete for biomedical applications. The incorporation of the porous structure may result in an enhanced degradation rate. The main advantage offer by the porous structure is to allow to flow the body transportation fluid through it and ease to proliferate the new tissue. Therefore, the current work focused on the development of a porous Fe structures using micro-extrusion based three-dimensional printing (ME3DP) and pressure less microwave sintering. The metallic-based polymeric ink used to fabricate the intent design structure. Subsequently, samples were heated in the microwave sintering furnace. The experimentations were done to evaluate the outcomes of different Fe concentrations (91–95 wt.%) on density and compressive yield strength of developed porous parts. Experimental observation deduced that fabricated part ≥ 94.wt.% of Fe concentration has strong bonding strength between the printed layers. Moreover, the mechanical property of 94 wt.% has found greater than 95 wt.% of Fe concentration. The scanning electron microscopic (SEM) image illustrated the presence of porous morphology into the fabricated body. Additionally, XRD (X-ray diffraction) plots exhibited the purity of sample without any contamination residue.","PeriodicalId":56519,"journal":{"name":"光:先进制造(英文)","volume":"9 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-08-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Experimental Investigation Into the Fabrication of Porous Biodegradable Fe Scaffold by Microwave Sintering of 3D Printed Green Body\",\"authors\":\"D. Mishra, P. M. Pandey\",\"doi\":\"10.1115/msec2021-63402\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"\\n Iron has appealing biodegradable properties that makes compatible for biodegradable implant tools applications. Although, the slow corrosion rate of Fe made obsolete for biomedical applications. The incorporation of the porous structure may result in an enhanced degradation rate. The main advantage offer by the porous structure is to allow to flow the body transportation fluid through it and ease to proliferate the new tissue. Therefore, the current work focused on the development of a porous Fe structures using micro-extrusion based three-dimensional printing (ME3DP) and pressure less microwave sintering. The metallic-based polymeric ink used to fabricate the intent design structure. Subsequently, samples were heated in the microwave sintering furnace. The experimentations were done to evaluate the outcomes of different Fe concentrations (91–95 wt.%) on density and compressive yield strength of developed porous parts. Experimental observation deduced that fabricated part ≥ 94.wt.% of Fe concentration has strong bonding strength between the printed layers. Moreover, the mechanical property of 94 wt.% has found greater than 95 wt.% of Fe concentration. The scanning electron microscopic (SEM) image illustrated the presence of porous morphology into the fabricated body. Additionally, XRD (X-ray diffraction) plots exhibited the purity of sample without any contamination residue.\",\"PeriodicalId\":56519,\"journal\":{\"name\":\"光:先进制造(英文)\",\"volume\":\"9 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-08-04\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"光:先进制造(英文)\",\"FirstCategoryId\":\"1087\",\"ListUrlMain\":\"https://doi.org/10.1115/msec2021-63402\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"光:先进制造(英文)","FirstCategoryId":"1087","ListUrlMain":"https://doi.org/10.1115/msec2021-63402","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

铁具有吸引人的可生物降解特性,使其与可生物降解植入工具的应用相兼容。尽管如此,铁的缓慢腐蚀速度使其在生物医学应用中过时了。多孔结构的掺入可以提高降解率。多孔结构提供的主要优点是允许身体运输液体通过它,并且易于新组织增殖。因此,目前的工作重点是利用基于微挤压的三维打印(ME3DP)和无压微波烧结技术开发多孔铁结构。用于制造意图设计结构的金属基聚合油墨。随后,样品在微波烧结炉中加热。研究了不同铁浓度(91 ~ 95 wt.%)对多孔件密度和抗压屈服强度的影响。实验观察推断,制件≥94.wt。%的铁浓度具有较强的印刷层之间的结合强度。此外,在94 wt.%的力学性能中发现了大于95 wt.%的铁浓度。扫描电镜(SEM)图像表明,在制备体中存在多孔形态。此外,XRD (x射线衍射)图显示样品纯度高,没有任何污染残留。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Experimental Investigation Into the Fabrication of Porous Biodegradable Fe Scaffold by Microwave Sintering of 3D Printed Green Body
Iron has appealing biodegradable properties that makes compatible for biodegradable implant tools applications. Although, the slow corrosion rate of Fe made obsolete for biomedical applications. The incorporation of the porous structure may result in an enhanced degradation rate. The main advantage offer by the porous structure is to allow to flow the body transportation fluid through it and ease to proliferate the new tissue. Therefore, the current work focused on the development of a porous Fe structures using micro-extrusion based three-dimensional printing (ME3DP) and pressure less microwave sintering. The metallic-based polymeric ink used to fabricate the intent design structure. Subsequently, samples were heated in the microwave sintering furnace. The experimentations were done to evaluate the outcomes of different Fe concentrations (91–95 wt.%) on density and compressive yield strength of developed porous parts. Experimental observation deduced that fabricated part ≥ 94.wt.% of Fe concentration has strong bonding strength between the printed layers. Moreover, the mechanical property of 94 wt.% has found greater than 95 wt.% of Fe concentration. The scanning electron microscopic (SEM) image illustrated the presence of porous morphology into the fabricated body. Additionally, XRD (X-ray diffraction) plots exhibited the purity of sample without any contamination residue.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
CiteScore
10.90
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信