R. Fuchs, S. Jost, H. Rudin, H.-J. Güntherodt, P. Fischer
{"title":"准晶和玻璃态Pd58.8Si20.6U20.6的制备及x射线和中子散射研究","authors":"R. Fuchs, S. Jost, H. Rudin, H.-J. Güntherodt, P. Fischer","doi":"10.1016/0025-5416(88)90371-0","DOIUrl":null,"url":null,"abstract":"<div><p>The metallic glass Pd<sub>58.8</sub>Si<sub>20.6</sub>U<sub>20.6</sub> has been produced by melt-spinning and was annealed in a helium stream at 790–805 K for 120–200 s.</p><p>During this procedure the material transforms into the so-called quasi-crystalline state. Differential scanning calorimetry (DSC) measurements have shown that more than 92% of the former metallic glass becomes quasi-crystalline, less than 1% is crystallized and the rest remains amorphous.</p><p>The data for elastic neutron and X-ray scattering are presented. The computed total structure factors are compared. In contrast to the X-ray results, the neutron measurements show no peaks below a scattering vector of 2 Å<sup>−1</sup>, which seems to indicate some chemical short-range order.</p></div>","PeriodicalId":100890,"journal":{"name":"Materials Science and Engineering","volume":"99 1","pages":"Pages 431-433"},"PeriodicalIF":0.0000,"publicationDate":"1988-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0025-5416(88)90371-0","citationCount":"0","resultStr":"{\"title\":\"Preparation and structural investigation by X-ray and neutron scattering of quasi-crystalline and glassy Pd58.8Si20.6U20.6\",\"authors\":\"R. Fuchs, S. Jost, H. Rudin, H.-J. Güntherodt, P. Fischer\",\"doi\":\"10.1016/0025-5416(88)90371-0\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>The metallic glass Pd<sub>58.8</sub>Si<sub>20.6</sub>U<sub>20.6</sub> has been produced by melt-spinning and was annealed in a helium stream at 790–805 K for 120–200 s.</p><p>During this procedure the material transforms into the so-called quasi-crystalline state. Differential scanning calorimetry (DSC) measurements have shown that more than 92% of the former metallic glass becomes quasi-crystalline, less than 1% is crystallized and the rest remains amorphous.</p><p>The data for elastic neutron and X-ray scattering are presented. The computed total structure factors are compared. In contrast to the X-ray results, the neutron measurements show no peaks below a scattering vector of 2 Å<sup>−1</sup>, which seems to indicate some chemical short-range order.</p></div>\",\"PeriodicalId\":100890,\"journal\":{\"name\":\"Materials Science and Engineering\",\"volume\":\"99 1\",\"pages\":\"Pages 431-433\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1988-03-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/0025-5416(88)90371-0\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Science and Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/0025541688903710\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Science and Engineering","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/0025541688903710","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Preparation and structural investigation by X-ray and neutron scattering of quasi-crystalline and glassy Pd58.8Si20.6U20.6
The metallic glass Pd58.8Si20.6U20.6 has been produced by melt-spinning and was annealed in a helium stream at 790–805 K for 120–200 s.
During this procedure the material transforms into the so-called quasi-crystalline state. Differential scanning calorimetry (DSC) measurements have shown that more than 92% of the former metallic glass becomes quasi-crystalline, less than 1% is crystallized and the rest remains amorphous.
The data for elastic neutron and X-ray scattering are presented. The computed total structure factors are compared. In contrast to the X-ray results, the neutron measurements show no peaks below a scattering vector of 2 Å−1, which seems to indicate some chemical short-range order.
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