具有分层孔隙率的新型陶瓷吸附剂和催化剂载体的合成

Tehnika Pub Date : 2023-01-01 DOI:10.5937/tehnika2303269k
Vesna Nikolić, J. Đokić, Denis Dinić, A. Marinković, Sanja Jevtić, Z. Anđić, Ž. Kamberović
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引用次数: 0

摘要

从工业的角度来看,多孔陶瓷是一种重要的材料,然而,经济上和技术上可接受的解决方案仍在寻求其制备。孔隙度控制是实现特定应用所需性能的关键步骤。为了获得多孔陶瓷,本工作采用高岭土和聚苯乙烯珠作为有机牺牲相。混合后,样品在1050℃下烧结1 h。表征包括傅里叶变换红外光谱(FTIR)、扫描电子显微镜(SEM)、x射线衍射分析(XRPD)、元素CHNS分析和抗压强度研究。对所得结果的分析表明,在有机组分的存在下,可以制备出层次有序、具有适当力学性能的多孔陶瓷,该有机组分在烧结过程中烧损后留下不同尺寸的孔隙。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of innovative ceramic sorbents and catalyst supports with hierarchical porosity
From an industrial point of view, porous ceramics represent an important material, however, economically and technologically acceptable solutions are still being sought for its preparation. Porosity control is a key step in achieving the desired properties for a specific application. In order to obtain multiporous ceramics, in this work, kaolin clay and polystyrene beads were used as organic sacrificial phase. After mixing, the samples were sintered at 1050 oC for 1 h. Characterization included Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), X-ray diffraction analysis (XRPD), elemental CHNS analysis and compressive strength investigations. The analysis of the obtained results showed that hierarchically ordered, multiporous ceramics, with appropriate mechanical properties can be prepared in the presence of an organic component whose burnout during sintering leaves behind pores of different dimensions.
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