银纳米粒子在BPSCCO超导薄膜上的合成与表征

S. Oboudi, M. Mustafa
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引用次数: 11

摘要

采用脉冲激光沉积(PLD)和沉积后氧退火技术在Si(111)衬底上生长了掺杂(Bi, Pb)-2223的外延银纳米颗粒薄膜。通过x射线衍射仪对合成膜的物相鉴定和总体结构特征进行了研究,结果表明所有样品均为正交晶型结构。采用标准的四探针法进行直流电阻率测量,结果表明,当银纳米颗粒增加到1.0 wt%时,Tc有所改善,这对所有研究薄膜的Tc都有最大的增强。通过扫描电镜(SEM)和原子力显微镜(AFM)对样品表面形貌进行了研究,结果表明,适当添加银纳米粒子可以增加样品中Tc的含量,从而促进Bi (Pb)-2223相的形成。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Ag Nanoparticles Addition on BPSCCO Superconducting Thin Films
The growth of epitaxial Ag nanoparticles doped (Bi, Pb)-2223 thin films on Si (111) substrates by pulsed laser deposition (PLD) and post-deposition oxygen annealing have been achieved. The phase identification and gross structural characteristics of synthesized films explored through X-ray diffractometer reveal that all the samples crystallize in orthorhombic structure. DC electrical resistivity measurements were done by the standard four-probe method and the results showed improvement in Tc by increasing Ag nanoparticles to 1.0 wt% which had a maximum enhancement in Tc for all investigated films. The surface morphology investigated through scanning electron microscope (SEM) and atomic force microscopy (AFM) results showed that an increase in Tc with the appropriate Ag nanoparticles addition in the samples is associated with the enhancement of Bi (Pb)-2223 phase formation.
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