浮力称重法测定水泥粒径分布

R. Tambun, N. Pratama, F. Hanum
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引用次数: 0

摘要

水泥粒度分布是水泥质量的重要特征之一。基于斯托克斯直径测量水泥粒径分布的简单方法有安德瑞森移液法、沉降天平法、离心沉降法等。这些方法的一个主要缺点是它们是耗时的过程,需要特殊的技能。粒度分布也可以用不同的原理通过显微镜、激光衍射/散射法和库尔特计数器法进行分析。即使这些方法在较短的时间内也能产生高度精确的结果,但设备昂贵。在目前的研究中,开发了一种新的方法来克服这个问题。方法为浮力称杆法。该方法简单,成本效益高。浮力称杆法的原理是通过对悬挂在悬浮液中的称杆称重浮力来测量颗粒迁移引起的悬浮液的密度变化,并利用称杆的长度和称杆表观质量的时程变化来计算颗粒的粒径分布。该仪器由一个分析天平和一个用于地板下称重的钩,以及一个用于检测悬浮液密度变化的称重棒组成。结果表明,浮力秤法适用于水泥粒径分布的测定,其结果与沉降秤法测定的结果相当。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Measurement of cement’s particle size distribution by the buoyancy weighing-bar method
One of the important characteristics of cement quality is particle size distribution. There are several simple methods to measure the particle size distribution of cement based on the Stokes diameter, like Andreasen pipette method, sedimentation balance method, centrifugal sedimentation method, etc. A major disadvantages of these methods are they are time consuming process and require special skills. Particle size distribution also can be analyzed by using a different principle through microscopy, laser diffraction/scattering methods and Coulter counter method. Even these  methods produce highly accurate results within a shorter time, however, the equipments are expensive. In the present study, it has developed a new method to overcome the problem. The method is the buoyancy weighing-bar method. This method is a simple and cost-effective. The principle of the buoyancy weighing-bar method that the density change in a suspension due to particle migration is measured by weighing buoyancy against a weighing–bar hung in the suspension, and the particle size distribution is calculated using the length of the weighing-bar and the time–course change in the the apparent mass of the weighing–bar. This apparatus consists of an analytical balance with a hook for underfloor weighing, and a weighing–bar, which is used to detect the density change in suspension. The result obtained show that the buoyancy weighing–bar method is suitable for measuring the particle size distribution of cement, and the result is comparable to that of determined by settling balance method.
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