{"title":"铜/氮化硅复合材料的制备与表征","authors":"M. A. Ahmed, W. Daoush, A. El-Nikhaily","doi":"10.12989/AMR.2016.5.3.131","DOIUrl":null,"url":null,"abstract":". Copper/silicon nitride (Cu/Si 3 N 4 ) composites are fabricated by powder technology process. Copper is used as metal matrix and very fine Si 3 N 4 particles (less than 1 micron) as reinforcement material. The investigated powder were used to prepare homogenous (Cu/Si 3 N 4 ) composite mixtures with different Si 3 N 4 weight percentage (2, 4, 6, 8 and10). The produced mixtures were cold pressed and sintered at different temperatures (850, 950, 1000, 1050 ° C). The microstructure and the chemical composition of the produced Cu/Si 3 N 4 composites were investigated by (SEM) and XRD. It was observed that the Si 3 N 4 particles were homogeneously distributed in the Cu matrix. The density, electrical conductivity and coefficient of thermal expansion of the produced Cu/Si 3 N 4 composites were measured. The relative green density, sintered density, electrical conductivity as well as coefficient of thermal expansion were decreased by increasing the reinforcement phase (Si 3 N 4 ) content in the copper matrix. It is also founded that the sintered density and electrical conductivity of the Cu/Si 3 N 4 composites were increased by increase the sintering temperature.","PeriodicalId":46242,"journal":{"name":"Advances in Materials Research-An International Journal","volume":null,"pages":null},"PeriodicalIF":1.9000,"publicationDate":"2016-09-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"5","resultStr":"{\"title\":\"Fabrication and characterization of Copper/Silicon Nitride composites\",\"authors\":\"M. A. Ahmed, W. Daoush, A. El-Nikhaily\",\"doi\":\"10.12989/AMR.2016.5.3.131\",\"DOIUrl\":null,\"url\":null,\"abstract\":\". Copper/silicon nitride (Cu/Si 3 N 4 ) composites are fabricated by powder technology process. Copper is used as metal matrix and very fine Si 3 N 4 particles (less than 1 micron) as reinforcement material. The investigated powder were used to prepare homogenous (Cu/Si 3 N 4 ) composite mixtures with different Si 3 N 4 weight percentage (2, 4, 6, 8 and10). The produced mixtures were cold pressed and sintered at different temperatures (850, 950, 1000, 1050 ° C). The microstructure and the chemical composition of the produced Cu/Si 3 N 4 composites were investigated by (SEM) and XRD. It was observed that the Si 3 N 4 particles were homogeneously distributed in the Cu matrix. The density, electrical conductivity and coefficient of thermal expansion of the produced Cu/Si 3 N 4 composites were measured. The relative green density, sintered density, electrical conductivity as well as coefficient of thermal expansion were decreased by increasing the reinforcement phase (Si 3 N 4 ) content in the copper matrix. It is also founded that the sintered density and electrical conductivity of the Cu/Si 3 N 4 composites were increased by increase the sintering temperature.\",\"PeriodicalId\":46242,\"journal\":{\"name\":\"Advances in Materials Research-An International Journal\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":1.9000,\"publicationDate\":\"2016-09-25\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"5\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Advances in Materials Research-An International Journal\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.12989/AMR.2016.5.3.131\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Advances in Materials Research-An International Journal","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.12989/AMR.2016.5.3.131","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
引用次数: 5
摘要
。采用粉末工艺制备了铜/氮化硅(Cu/ si3n4)复合材料。铜作为金属基体,非常细的Si 3n4颗粒(小于1微米)作为增强材料。用所研究的粉末制备了不同Si 3 N 4重量百分比(2、4、6、8和10)的均相(Cu/Si 3 N 4)复合混合物。采用不同温度(850、950、1000、1050℃)对制备的Cu/ si3n4复合材料进行冷压和烧结,并采用SEM和XRD分析制备的Cu/ si3n4复合材料的微观结构和化学成分。结果表明,si3n4颗粒均匀分布在Cu基体中。测定了制备的Cu/ si3n4复合材料的密度、电导率和热膨胀系数。增加铜基体中增强相(si3n4)的含量,降低了相对生坯密度、烧结密度、电导率和热膨胀系数。随着烧结温度的升高,Cu/ si3n4复合材料的烧结密度和电导率均有所提高。
Fabrication and characterization of Copper/Silicon Nitride composites
. Copper/silicon nitride (Cu/Si 3 N 4 ) composites are fabricated by powder technology process. Copper is used as metal matrix and very fine Si 3 N 4 particles (less than 1 micron) as reinforcement material. The investigated powder were used to prepare homogenous (Cu/Si 3 N 4 ) composite mixtures with different Si 3 N 4 weight percentage (2, 4, 6, 8 and10). The produced mixtures were cold pressed and sintered at different temperatures (850, 950, 1000, 1050 ° C). The microstructure and the chemical composition of the produced Cu/Si 3 N 4 composites were investigated by (SEM) and XRD. It was observed that the Si 3 N 4 particles were homogeneously distributed in the Cu matrix. The density, electrical conductivity and coefficient of thermal expansion of the produced Cu/Si 3 N 4 composites were measured. The relative green density, sintered density, electrical conductivity as well as coefficient of thermal expansion were decreased by increasing the reinforcement phase (Si 3 N 4 ) content in the copper matrix. It is also founded that the sintered density and electrical conductivity of the Cu/Si 3 N 4 composites were increased by increase the sintering temperature.