Partially melted powder in laser based directed energy deposition: Formation mechanism and its influence on microstructure

The powder–melt pool interaction behavior is crucial in laser-based directed energy deposition (LDED). Partially melted particles, which are formed as a result of this interaction, significantly influence on the microstructure and mechanical performance of multi-material and metal-matrix composites fabricated via LDED. However, the presence of partially melted particles is a contentious issue that has been overlooked in single-material LDED studies. Furthermore, the investigation of partially melted particles is hindered by the difficulties in direct observation. To overcome this obstacle, this study was conducted using a single-bead Ti–6Al–4V printing experiment with a relatively high oxygen content to distinguish partially melted particles directly. The formation mechanism of the partially melted particles was revealed through experimental studies combined with numerical analysis using a self-established model. Additionally, the influence of partially melted particles on the grain structure of LDED–fabricated parts was investigated in a low–oxygen environment. The partially melted particles tend to survive close to the surface of the deposited layer. As the penetration depth increased, the particle size decreased and the aspect ratio increased. The formation of partially melted particles collectively depends on the laser power, scanning velocity, powder size and powder feed speed, differing from the common conclusion that an insufficient input energy results in poor powder melting behavior. Furthermore, a Ti–6Al–4V sample with high–fraction equiaxed grains was fabricated using optimized processing conditions. The partially melted particles significantly affected the solidification behavior. In addition to the heterogeneous nucleation mechanism caused by the partially melted particles, a novel seed crystal mechanism was proposed to support the abnormal formation of equiaxed grains. This study highlights the importance of partially melted particles in LDED, and provides useful insights into in-situ microstructural control in LDED.