绿色合成纳米银用于超滤膜表面改性及抗菌活性研究

Hansnath Tiwari , Kulbhushan Samal , Sachin Rameshrao Geed , Sounak Bera , Chandan Das , Kaustubha Mohanty
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引用次数: 0

摘要

本研究介绍了生物合成的银纳米颗粒(AgNPs)在超滤膜表面改性以赋予抗菌性能方面的应用。以药用植物木犀叶提取物为原料合成了AgNPs,并利用紫外光谱、红外光谱、X射线衍射、FESEM、HRTEM和原子力显微镜对其进行了表征。合成AgNPs的最佳条件是反应时间为240分钟,pH为9.5,前体与生物提取物的初始浓度为1:1(v/v),温度为323K。发现合成的AgNPs是平均尺寸为20nm的球形,并且本质上是结晶的。然后使用浸涂技术将AgNP沉积在平片聚醚砜(PES)膜(MWCO 30kDa)上。使用FESEM和EDX分析证实了AgNPs在膜表面的沉积。所得到的掺入AgNPs的膜显示出对大肠杆菌的有效抗菌活性。这些发现突出了生物合成的AgNPs在开发具有抗菌性能的功能化超滤膜方面的潜力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Green synthesis of silver nanoparticles for ultrafiltration membrane surface modification and antimicrobial activity

Green synthesis of silver nanoparticles for ultrafiltration membrane surface modification and antimicrobial activity

This study presents the application of biosynthesized silver nanoparticles (AgNPs) for modifying the surface of ultrafiltration membranes to confer antimicrobial properties. The AgNPs were synthesized using leaf extract of the medicinal plant Mimusops elengi L, and their characterization was carried out using UV spectroscopy, FTIR, XRD, FESEM, HRTEM, and AFM analyses. The optimal conditions for the synthesis of AgNPs were determined to be 240 min of reaction time, pH 9.5, 1:1 (v/v) ratio of initial concentration of precursor to bio-extract, and 323 K temperature. The synthesized AgNPs were found to be spherical with an average size of 20 nm and crystalline in nature. The AgNPs were then deposited on flat sheet polyether sulfone (PES) membranes (MWCO 30 kDa) using the dip coating technique. The deposition of AgNPs on the membrane surface was confirmed using FESEM and EDX analysis. The resulting AgNPs-incorporated membrane demonstrated effective antibacterial activity against E.coli. These findings highlight the potential of biosynthesized AgNPs for developing functionalized ultrafiltration membranes with antimicrobial properties.

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