乙醇-盐酸萃取芒果皮花青素的传质系数

Eksergi Pub Date : 2022-11-13 DOI:10.31315/e.v19i3.8008
Zubaidi Achmad, Faizah Hadi, S. Kholisoh
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引用次数: 0

摘要

花青素是一种天然色素,可导致山竹果实的紫色表皮。本研究旨在观察温度、搅拌时间和乙醇-盐酸溶剂中乙醇浓度对山竹皮提取过程中产生的花青素的影响,并测定其传质系数。使用提取装置组,用含有1%HCl溶液的乙醇溶剂提取山竹皮粉末进行实验室工作。将山竹皮清洗干净,然后捣碎,直到它达到-60+80目的大小。然后将50g山竹皮粉末与各种浓度为55%、65%、75%、85%和95%的乙醇溶液一起放入三颈烧瓶中,每个乙醇溶液含有1%HCl。萃取在3、4、5、6和7小时的不同搅拌时间下进行,温度变化为30、40、50、60和70℃。每种产品在<60℃的温度下蒸馏。采用分光光度法测定花青素含量。结果表明,在提取温度为50℃、搅拌时间为4小时、乙醇浓度为95%的乙醇-盐酸溶剂中,花青素含量为98377.10-4(g花青素/g溶剂),kC为000781 g/(cm2.hour)的最佳条件下。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Mass Transfer Coefficient of Extraction of Anthocyanin from Mangosteen Peel (Garcinia mangostana L.) with Ethanol-HCl as Solvent
Anthocyanin is a natural pigment that causes the purple skin of the mangosteen fruit. This study aimed to observe the effect of temperature, stirring time, and ethanol concentration in ethanol–HCl solvent on anthocyanins produced from the mangosteen peel extraction process and determine the value of its mass transfer coefficient. The laboratory work was conducted with mangosteen peel powder extracted with ethanol solvent containing 1% HCl solution using an extraction apparatus set. The mangosteen rind is cleaned and then mashed until it passes the size of -60+80 mesh. Then 50 g of mangosteen rind powder was put into a three-neck flask along with ethanol solution with various concentrations of 55%, 65%, 75%, 85%, and 95%, each containing 1% HCl. Extraction was carried out at various stirring times of 3, 4, 5, 6, and 7 hours with temperature variations of 30, 40, 50, 60, and 70oC. Each product was distilled at a temperature of <60oC. Anthocyanin content were analyzed by spectrophotometric method. The results showed that the optimum conditions at the extraction temperature of 50oC with stirring time for 4 hours and 95% ethanol concentration in ethanol–HCl solvent with anthocyanin content obtained of 9,8377.10-4 (g anthocyanin/g solvent) and kC of 0,00781 g/(cm2.hour).
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