N1-（3,5-双（三氟甲基）苄基）苯-1,2-二胺和N，N-双（2-硝基苯基）-3,5-双（三氟甲基）苯胺的合成

IF 0.6 Q4 CHEMISTRY, ORGANIC

Molbank Pub Date : 2023-09-04 DOI:10.3390/m1718

Luka Ciber, Helena Brodnik, F. Požgan, J. Svete, B. Štefane, Uroš Grošelj

引用次数: 0

摘要

由市售的3，5-双（三氟甲基）苄胺和1-氟-2-硝基苯分两步制备单取代的苯-1，2-二胺构建基块，N1-（3，5-二（三氟甲酯）苄基）苯-1，2二胺，同时使用3，5-两（三氟甲基）苯胺作为起始胺得到三芳基胺，N，N-双（2-硝基苯基）-3，5-双三氟甲基苯胺。对新合成的化合物进行了结构表征。

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Synthesis of N1-(3,5-Bis(trifluoromethyl)benzyl)benzene-1,2-diamine and N,N-Bis(2-nitrophenyl)-3,5-bis(trifluoromethyl)aniline

A monosubstituted benzene-1,2-diamine building block, N1-(3,5-bis(trifluoromethyl)benzyl)benzene-1,2-diamine, was prepared in two steps from commercially available 3,5-bis(trifluoromethyl)benzylamine and 1-fluoro-2-nitrobenzene, while the use of 3,5-bis(trifluoromethyl)aniline as the starting amine gave a triarylamine, N,N-bis(2-nitrophenyl)-3,5-bis(trifluoromethyl)aniline. The structures of the newly synthesized compounds were fully characterized.

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来源期刊

Molbank Chemistry-Physical and Theoretical Chemistry

CiteScore

0.70

自引率

33.30%

发文量

174

审稿时长

11 weeks

期刊介绍： •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)