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Q3 Biochemistry, Genetics and Molecular Biology

Current protocols in chemical biology Pub Date : 2019-06-13 DOI:10.1002/cpch.55

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摘要

封面:Liu et al. (https://doi.org/10.1002/cpch.64)， (A)在96孔板中使用饱和SO2F2溶液对苯酚进行氟磺化。(B)用结晶盐1-(氟硫酰基)-2,3-二甲基- 1h -咪唑-3-ium三氟甲烷磺酸氟磺化苯酚、仲胺和伯胺。在不同的反应条件下，分别得到芳基氟磺酸盐、磺酰氟和nh -磺酰氟(或双(氟磺酰)亚胺)。看到e64。

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Cover: In Liu et al. (https://doi.org/10.1002/cpch.64), (A) Fluorosulfurylation of phenols using saturated SO₂F₂ solution in a 96-well plate. (B) Fluorosulfurylation of phenols, secondary amines, and primary amines with the crystalline salt 1-(fluorosulfuryl)-2,3-dimethyl-1H-imidazol-3-ium trifluoromethanesulfonate. Arylfluorosulfates, sulfamoyl fluorides, and NH-sulfamoyl fluorides (or bis(fluorosulfuryl)imide, with different reaction conditions) are respectively obtained. See e64.

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Current protocols in chemical biology Biochemistry, Genetics and Molecular Biology-Biophysics

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