纳米红宝石的制备与表征

Q4 Chemistry
W. Razali, A. Kasim, S. A. Senawi, A. Hashim, N. Yahya, H. A. Rafaie
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引用次数: 3

摘要

在寻找具有优异光学性能的纳米颗粒(NP)方面已经做了许多工作。在这项工作中,使用飞秒激光烧蚀制备了红宝石(铬掺杂氧化铝)纳米颗粒。利用动态光散射(DLS)、透射电子显微镜(TEM)和荧光显微镜对合成的纳米颗粒进行了表征。DLS分析表明,颗粒尺寸约为52nm。与DLS分析相比,TEM分析给出了平均尺寸为38nm的较小颗粒尺寸。通过透射电镜观察到颗粒呈球形。合成的纳米粒子在具有+55mVζ电位值的水中表现出优异的稳定性。激发红宝石NP的最有效波长被确定为405nm和554nm。红宝石NP的发射峰在690nm处,这对应于2E-4A2跃迁。合成的红宝石纳米颗粒可作为潜在的生物成像标记物
本文章由计算机程序翻译,如有差异,请以英文原文为准。
FABRICATION AND CHARACTERIZATION OF RUBY NANOPARTICLES
Numerous works have been done on finding nanoparticles (NPs) with excellent optical properties. In this work, ruby (chromium doped alumina) nanoparticles have been prepared using femtosecond laser ablation. The synthesized nanoparticles were characterised using dynamic light scattering (DLS), transmission electron microscopy (TEM) and fluorescence microscopy. DLS analysis indicates that the particles size is approximately 52 nm. TEM analysis gives smaller particles size with mean size of 38 nm compared to DLS analysis. Spherical shape of the particles was observed through TEM image. The synthesized NPs showed excellent stability in water with +55 mV zeta potential value. The most efficient wavelengths to excite the ruby NPs were determined as 405 nm and 554 nm. The emission peak for the ruby NPs was at 690 nm which is corresponds to 2E-4A2 transition. The synthesized ruby NPs can be applied as a potential bioimaging label
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来源期刊
Malaysian Journal of Analytical Sciences
Malaysian Journal of Analytical Sciences Chemistry-Analytical Chemistry
CiteScore
1.10
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