2-氧-1,2-二氢喹啉-8-酰基4-氯苯甲酸酯的合成、光谱和热分析

IF 0.6 Q4 CHEMISTRY, ORGANIC

Molbank Pub Date : 2023-06-19 DOI:10.3390/m1672

Diana Becerra, Hugo Rojas, J. Castillo

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引用次数: 0

摘要

采用三乙胺介导的8-羟基喹啉-2（1H）-酮与4-氯苯甲酰氯在乙腈中的O-酰化反应，在室温下合成了2-氧代-1,2-二氢喹啉-8-基4-氯苯甲酸酯。这种方法以其干净的反应曲线和简单的程序而闻名。通过光谱、光谱和热分析对2-氧代喹啉衍生物进行了表征，从而能够全面了解其分子结构和热性能。

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Synthesis, Spectroscopic, and Thermal Analyses of 2-Oxo-1,2-dihydroquinolin-8-yl 4-chlorobenzoate

The 2-oxo-1,2-dihydroquinolin-8-yl 4-chlorobenzoate was synthesized in good yield using a triethylamine-mediated O-acylation reaction between 8-hydroxyquinolin-2(1H)-one and 4-chlorobenzoyl chloride in acetonitrile at room temperature. This methodology is notable for its clean reaction profile and straightforward procedure. The 2-oxoquinoline derivative was characterized using spectroscopic, spectrometric, and thermal analyses, enabling a comprehensive understanding of its molecular structure and thermal properties.

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来源期刊

Molbank Chemistry-Physical and Theoretical Chemistry

CiteScore

0.70

自引率

33.30%

发文量

174

审稿时长

11 weeks

期刊介绍： •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)