{"title":"用DBU合成RAFT聚合链转移剂","authors":"S. Gondi","doi":"10.33774/chemrxiv-2021-sf0t0","DOIUrl":null,"url":null,"abstract":"Trithiocarbonate TTC, Dithioester DT containing RAFT chain transfer acid agents are efficiently and conveniently esterified by DBU. The significance of the reaction is mild reaction condition, high yield, easy simple workup, and reduction of reaction time. This protocol providing a useful alternative method for ester synthesis and makes the process very viable or more economic.","PeriodicalId":72565,"journal":{"name":"ChemRxiv : the preprint server for chemistry","volume":" ","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2021-09-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of Chain Transfer Agents for RAFT Polymerization by using DBU\",\"authors\":\"S. Gondi\",\"doi\":\"10.33774/chemrxiv-2021-sf0t0\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Trithiocarbonate TTC, Dithioester DT containing RAFT chain transfer acid agents are efficiently and conveniently esterified by DBU. The significance of the reaction is mild reaction condition, high yield, easy simple workup, and reduction of reaction time. This protocol providing a useful alternative method for ester synthesis and makes the process very viable or more economic.\",\"PeriodicalId\":72565,\"journal\":{\"name\":\"ChemRxiv : the preprint server for chemistry\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-09-16\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"ChemRxiv : the preprint server for chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.33774/chemrxiv-2021-sf0t0\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"ChemRxiv : the preprint server for chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.33774/chemrxiv-2021-sf0t0","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Synthesis of Chain Transfer Agents for RAFT Polymerization by using DBU
Trithiocarbonate TTC, Dithioester DT containing RAFT chain transfer acid agents are efficiently and conveniently esterified by DBU. The significance of the reaction is mild reaction condition, high yield, easy simple workup, and reduction of reaction time. This protocol providing a useful alternative method for ester synthesis and makes the process very viable or more economic.
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