绿色生物合成氧化银纳米颗粒Ag2O的新方法、表征及催化应用

IF 1.3 Q3 ENGINEERING, CHEMICAL
Brahim El-Ghmari, H. Farah, Abdellah Ech-chahad
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引用次数: 11

摘要

本文以野生植物Herniaria hirsuta (H. hirsuta)的提取物为原料,采用简便、绿色的方法合成氧化银纳米颗粒Ag2O NPs。采用不同的光谱方法对生物合成的Ag2O NPs进行表征,紫外-可见(UV-Vis)光谱得到Ag2O NPs的表面等离子体共振(SPR)峰为430 nm,直接禁带和间接禁带分别为3.76 eV和3.68 eV;傅里叶变换红外(FTIR)光谱分析揭示了Ag2O NPs的稳定性和合成的基团。扫描电镜(SEM)研究了Ag2O NPs的形貌,发现Ag2O NPs呈近球形,x射线衍射(XRD)研究证实了Ag2O NPs的结晶度为15.51 nm。通过对亚甲基蓝染料的降解,研究了Ag2O NPs的催化活性和环数。版权所有©2021作者,BCREC集团出版。这是一篇基于CC BY-SA许可(https://creativecommons.org/licenses/by-sa/4.0)的开放获取文章。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
A New Approach for the Green Biosynthesis of Silver Oxide Nanoparticles Ag2O, Characterization and Catalytic Application
In this paper, a facile and green approach for the synthesis of silver oxide nanoparticles Ag2O NPs was performed using the extract of the wild plant Herniaria hirsuta (H. hirsuta). Different spectral methods were used for the characterization of the biosynthesized Ag2O NPs, ultraviolet-visible (UV-Vis) spectroscopy gave a surface plasmon resonance (SPR) peak of Ag2O NPs is 430 nm, estimation of direct and indirect forbidden gap bands are respectively 3.76 eV and 3.68 eV; Fourier transform infrared (FTIR) spectral analysis revealed the groups responsible for the stability and synthesis of Ag2O NPs. The morphology of Ag2O NPs was studied by scanning electron microscopy (SEM) showing a nearly spherical shape of Ag2O NPs, and X-ray diffraction (XRD) study confirmed the crystallinity of Ag2O NPs with a crystallinity size of 15.51 nm. The catalytic activity of Ag2O NPs, as well as the rings number were studied by the degradation of methylene blue dye. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).
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来源期刊
CiteScore
3.20
自引率
6.70%
发文量
52
审稿时长
12 weeks
期刊介绍: Bulletin of Chemical Reaction Engineering & Catalysis, a reputable international journal, provides a forum for publishing the novel technologies related to the catalyst, catalysis, chemical reactor, kinetics, and chemical reaction engineering. Scientific articles dealing with the following topics in chemical reaction engineering, catalysis science and engineering, catalyst preparation method and characterization, novel innovation of chemical reactor, kinetic studies, etc. are particularly welcome. However, articles concerned on general chemical engineering process are not covered and out of scope of this journal
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