陶瓷改性与树脂改性玻璃离子体修复材料的断裂韧性、硬度和微观结构

Ibrahim M. Hamouda
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摘要

本研究的目的是评估和比较陶瓷改性与树脂改性玻璃离聚物修复材料的断裂韧性、硬度和微观结构。对于断裂韧性,在不锈钢分模(25mm长、2.5mm厚和5mm宽)中制作了20个来自这两种材料的试样。使用Lloyd万能试验机以2mm/min的十字头速度测量断裂韧性。为了进行硬度测试,在圆盘形不锈钢模具(直径5毫米,高度2毫米)中制作了两种材料的20个试样。所有样品均在37°C的蒸馏水中储存24小时。使用维氏显微硬度计在50g载荷下测量硬度。使用扫描电子显微镜检查了这两种材料的微观结构。研究结果表明,两种材料的断裂韧性没有显著差异。陶瓷改性玻璃离聚物的硬度高于树脂改性型。在玻璃离聚物中加入陶瓷填料并没有提高其断裂韧性。树脂改性玻璃离聚物的微观结构显示基体与树脂填料之间紧密堆积,而陶瓷改性玻璃离聚物显示基体与陶瓷填料分离。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Fracture Toughness, Hardness, and Microstructure of Ceramic Modified Versus Resin Modified Glass Ionomer Restorative Materials
The aim of this study was evaluation and comparison of fracture toughness, hardness and microstructure of ceramic-modified versus resin-modified glass ionomer restorative materials. For fracture toughness, 20 specimens from both materials were fabricated in a stainless-steel split mold (25mm length, 2.5mm thickness and 5mm width). Fracture toughness was measured using Lloyd universal testing machine with cross head speed 2 mm/min. For hardness testing, 20 specimens from both materials were fabricated in a disc-shaped stainless-steel mold (5mm diameter and 2mm height). All specimens were stored in distilled water at 37°C for 24 hours. Hardness was measured using Vickers micro hardness tester with 50 g load. The microstructure of both materials was examined using scanning electron microscopy. The results of this study showed there wasn’t significant difference between both materials in fracture toughness. The hardness of ceramic-modified glass ionomer was higher than that of the resin-modified type. The addition of ceramic filler to the glass ionomer didn’t improve its fracture toughness. The microstructure of resin-modified glass ionomer showed tight packing between the matrix and the resin filler, while the ceramic-modified glass ionomer showed separated matrix from the ceramic filler.
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