{"title":"动态温湿度箱在生物材料吸湿等温线测量中的应用与传统等静压法的比较","authors":"Maha Al-Khalili, N. Al-Habsi, M. Rahman","doi":"10.1155/2021/1236427","DOIUrl":null,"url":null,"abstract":"Measurement of water activity and moisture sorption isotherms of foods and biomaterials are important to determine the state of water. In this work, a dynamic temperature-humidity (DTH) controlled chamber was used to measure water sorption isotherm and compared with the conventional isopiestic method. Temperature and relative humidity of DTH chamber can be controlled in the range of -15 to 100°C and 0 to 98%, respectively; thus, measurement of water activity at any point can be measured within the above ranges. The DTH chamber method showed high reproducibility as compared with the conventional isopiestic method when measured isotherms of cellulose, lignin, and hemicellulase were compared at 30°C. Finally, isotherm data of cellulose, lignin, and hemicellulase were generated in the temperature range of 10-90°C using DTH chamber, and these were modelled by BET and GAB equations. The model parameters were correlated with the temperature.","PeriodicalId":7315,"journal":{"name":"Adsorption Science & Technology","volume":" ","pages":""},"PeriodicalIF":2.8000,"publicationDate":"2021-12-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Application of Dynamic Temperature-Humidity Chamber for Measuring Moisture Sorption Isotherms of Biomaterials as Compared to the Conventional Isopiestic Method\",\"authors\":\"Maha Al-Khalili, N. Al-Habsi, M. Rahman\",\"doi\":\"10.1155/2021/1236427\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Measurement of water activity and moisture sorption isotherms of foods and biomaterials are important to determine the state of water. In this work, a dynamic temperature-humidity (DTH) controlled chamber was used to measure water sorption isotherm and compared with the conventional isopiestic method. Temperature and relative humidity of DTH chamber can be controlled in the range of -15 to 100°C and 0 to 98%, respectively; thus, measurement of water activity at any point can be measured within the above ranges. The DTH chamber method showed high reproducibility as compared with the conventional isopiestic method when measured isotherms of cellulose, lignin, and hemicellulase were compared at 30°C. Finally, isotherm data of cellulose, lignin, and hemicellulase were generated in the temperature range of 10-90°C using DTH chamber, and these were modelled by BET and GAB equations. The model parameters were correlated with the temperature.\",\"PeriodicalId\":7315,\"journal\":{\"name\":\"Adsorption Science & Technology\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":2.8000,\"publicationDate\":\"2021-12-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Adsorption Science & Technology\",\"FirstCategoryId\":\"5\",\"ListUrlMain\":\"https://doi.org/10.1155/2021/1236427\",\"RegionNum\":4,\"RegionCategory\":\"工程技术\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"CHEMISTRY, APPLIED\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Adsorption Science & Technology","FirstCategoryId":"5","ListUrlMain":"https://doi.org/10.1155/2021/1236427","RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"CHEMISTRY, APPLIED","Score":null,"Total":0}
Application of Dynamic Temperature-Humidity Chamber for Measuring Moisture Sorption Isotherms of Biomaterials as Compared to the Conventional Isopiestic Method
Measurement of water activity and moisture sorption isotherms of foods and biomaterials are important to determine the state of water. In this work, a dynamic temperature-humidity (DTH) controlled chamber was used to measure water sorption isotherm and compared with the conventional isopiestic method. Temperature and relative humidity of DTH chamber can be controlled in the range of -15 to 100°C and 0 to 98%, respectively; thus, measurement of water activity at any point can be measured within the above ranges. The DTH chamber method showed high reproducibility as compared with the conventional isopiestic method when measured isotherms of cellulose, lignin, and hemicellulase were compared at 30°C. Finally, isotherm data of cellulose, lignin, and hemicellulase were generated in the temperature range of 10-90°C using DTH chamber, and these were modelled by BET and GAB equations. The model parameters were correlated with the temperature.
期刊介绍:
Adsorption Science & Technology is a peer-reviewed, open access journal devoted to studies of adsorption and desorption phenomena, which publishes original research papers and critical review articles, with occasional special issues relating to particular topics and symposia.