电感耦合等离子体磁控溅射增强CrN膜的耐蚀性

IF 0.8 Q4 ELECTROCHEMISTRY
S. Chun, Seong-Jong Kim
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引用次数: 0

摘要

电感耦合等离子体磁控溅射(ICPMS)的优点是通过提高等离子体电离率和沉积过程中的离子轰击效应,可以显著改善涂层的性能。因此,本文比较了直流磁控溅射(dcMS)和ICPMS系统沉积CrN薄膜的结果。通过x射线衍射、扫描电镜、纳米压痕和耐蚀性测试研究了CrN涂层的结构、微观结构、机械性能和腐蚀性能。ICPMS沉积的CrN薄膜在200平面上的生长优于在111平面上的生长。结果表明,ICPMS沉积的薄膜微观结构紧凑,硬度高。纳米压痕硬度达到19.8 GPa, dcMS测定硬度为13.5 GPa。ICPMS法制备CrN膜的腐蚀电流密度约为9.8 × 10 -6 mA/cm 2,是dcMS法制备CrN膜的腐蚀电流密度4.6 × 10 -3 mA/cm 2的1/470。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Enhancement of the Corrosion Resistance of CrN Film Deposited by Inductively Coupled Plasma Magnetron Sputtering
Inductively coupled plasma magnetron sputtering (ICPMS) has the advantage of being able to dramatically improve coating properties by increasing the plasma ionization rate and the ion bombardment effect during deposition. Thus, this paper presents the comparative results of CrN films deposited by direct current magnetron sputtering (dcMS) and ICPMS systems. The structure, microstructure, and mechanical and corrosive properties of the CrN coatings were investigated by X-ray diffractometry, scanning electron microscopy, nanoindentation, and corrosion-resistance measurements. The as-deposited CrN films by ICPMS grew preferentially on a 200 plane compared to dcMS on a 111 plane. As a result, the films deposited by ICPMS had a very compact microstructure with high hardness. The nanoindentation hardness reached 19.8 GPa, and 13.5 GPa by dcMS. The corrosion current density of CrN film prepared by ICPMS was about 9.8 × 10 -6 mA/cm 2 , which was 1/470 of 4.6 × 10 -3 mA/cm 2 , the corrosion current density of CrN film prepared by dcMS.
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来源期刊
CiteScore
1.30
自引率
66.70%
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