超弹性材料应变损伤的扫描电子显微镜分析:一种基于数字图像处理的统计方法

IF 3.2 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Md Moonim Lateefi, Firozut Tauheed, Somnath Sarangi
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引用次数: 0

摘要

为了获得比普通光学显微镜具有更好的分辨率和聚焦深度的地形/形态图像,使用扫描电子显微镜(SEM)在所需的点上拍摄材料或样品表面的照片。在聚合物和橡胶材料科学的背景下,扫描电镜研究经常试图可视化相形态、表面和横截面形貌以及表面分子秩序,并阐明损伤机制。在橡胶硫化胶的情况下,测试样品经常通过各种机械性能评估程序,包括拉伸,弯曲,疲劳,磨损和撕裂测试,以最终确定所需质量水平的复合参数。试件的损伤表面表现出独特的地形特征,这些特征被捕获为扫描电镜图像,并与相关的强度特性相关联。然而,大多数情况下,强度属性与表面形貌类型之间的关系是定性的。表面粗糙度测量指标,如均方根(r.m.s)粗糙度、平均粗糙度和峰谷距离,经常使用SEM中可访问的标准软件来确定定量研究。本研究的主要目标是使用基于统计/光谱的技术,利用扫描电镜定量测量表面形貌。用一个现象模型预测了一种各向同性、不可压缩、超弹性类橡胶材料的Mullins应力软化现象。该模型采用简单的指数损伤函数表征了类橡胶材料变形引起的微观结构退化。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Strain-induced damage analysis of hyperelastic material through scanning electron microscopy: A statistical approach using digital image processing

In order to acquire topographic/morphological images with superior resolution and depth of focus than an ordinary optical microscope, scanning electron microscopy (SEM) is used to take photographs of a surface of materials or specimens at a desired point. In the context of polymer and rubber materials science, SEM investigations frequently try to visualize phase morphology, surface and cross-sectional topography, and surface molecular order, and clarify damage mechanisms. In the case of rubber vulcanizates, test specimens are frequently put through a variety of mechanical property assessment procedures, including tensile, flexing, fatigue, abrasion, and tear tests, in order to finalize compounding parameters for required levels of quality. The damaged surface of the test specimens exhibits distinctive topographical characteristics, which are captured as an SEM picture and associated with relevant strength properties. However, the majority of the time, the relationship between strength attributes and the type of surface topography is qualitative. Surface roughness measurement metrics such as root mean square (r.m.s) roughness, average roughness, and peak-to-valley distance are frequently determined for quantitative research using standard software accessible in an SEM. The primary goal of this research is to use a statistical/spectral-based technique for quantitatively measuring surface topography using SEM. The Mullins stress-softening phenomenon of an isotropic, incompressible, hyperelastic rubberlike material is predicted using a phenomenological model. A simple exponential damage function characterizes the model, which represents deformation-induced microstructural degradation of rubberlike material.

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来源期刊
Forces in mechanics
Forces in mechanics Mechanics of Materials
CiteScore
3.50
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