(2 z, 5 z) 5 - ((3 - (Benzofuran-2-yl) 1-phenyl-1h-pyrazol-4-yl)亚甲基)- 2 - ((4-methoxyphenyl)亚氨基的)3-phenylthiazolidin-4-one

IF 0.6 Q4 CHEMISTRY, ORGANIC

Molbank Pub Date : 2023-06-09 DOI:10.3390/m1665

Bakr F. Abdel-Wahab, Hanan A. Mohamed, Benson M. Kariuki, Gamal A. El-Hiti

引用次数: 0

摘要

3-（苯并呋喃-2-基）-1-苯基-1H-吡唑-4-甲醛（1）和2-（（4-甲氧基苯基）亚氨基）-3-苯基噻唑烷-4-酮（2）在含有哌啶作为催化剂的无水乙醇中的1:1混合物在回流下反应4小时，得到（2Z，5Z）-5-（（（3-（苯并呋喃-2-基]-1-苯基-1H吡唑-4-基）亚甲基）-2-（（4-甲基苯基）亚氨基）-3-苯基吡唑-4-酮（3），C34H24N4O3F，产率82%。通过X射线衍射和光谱分析证实了新合成的杂环的结构。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

查看原文本刊更多论文

(2Z,5Z)-5-((3-(Benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl)methylene)-2-((4-methoxyphenyl)imino)-3-phenylthiazolidin-4-one

The reaction of a 1:1 mixture of 3-(benzofuran-2-yl)-1-phenyl-1H-pyrazole-4-carbaldehyde (1) and 2-((4-methoxyphenyl)imino)-3-phenylthiazolidin-4-one (2) in anhydrous ethanol containing piperidine as a catalyst under reflux for 4 h gave (2Z,5Z)-5-((3-(benzofuran-2-yl)-1-phenyl-1H-pyrazol-4-yl)methylene)-2-((4-methoxyphenyl)imino)-3-phenylthiazolidin-4-one (3), C34H24N4O3F, in 82% yield. The structure of the newly synthesized heterocycle was confirmed via X-ray diffraction and spectral analyses.

求助全文

通过发布文献求助，成功后即可免费获取论文全文。去求助

来源期刊

Molbank Chemistry-Physical and Theoretical Chemistry

CiteScore

0.70

自引率

33.30%

发文量

174

审稿时长

11 weeks

期刊介绍： •organic synthesis •biosynthesis •extraction and purification •natural product derivatives •structural elucidation (X-ray crystallography, NMR, etc.)