用树楸树皮水萃取物环保合成纳米银

N. Azis, A. Wahab, A. Karim, N. La Nafie, Triana Febrianti
{"title":"用树楸树皮水萃取物环保合成纳米银","authors":"N. Azis, A. Wahab, A. Karim, N. La Nafie, Triana Febrianti","doi":"10.14710/jksa.25.6.224-230","DOIUrl":null,"url":null,"abstract":"In this present study, silver nanoparticles (AgNPs) were synthesized through an easy, rapid, and eco-friendly pathway using Lannea coromandelica aqueous bark extract. The obtained AgNPs were characterized using Ultraviolet-Visible (UV-Vis) spectrophotometer, Fourier Transform Infrared (FTIR), X-ray Diffraction (XRD), and Scanning Electron Microscope (SEM). The results indicated that the pH of colloidal AgNPs played a vital role in forming AgNPs. The pH ranges used in this study were 6, 8, 10, and 12. The formation of AgNPs was confirmed by observing the surface plasmon resonance (SPR) band at each pH and obtaining a wavelength of 430.50, 419.50, 418.50, and 410.00 nm. A comparison of the FTIR spectra of Lannea coromandelica aqueous bark extract and AgNPs showed the contribution of the O-H group in reducing silver ions. XRD diffractogram showed that AgNPs formed at 2θ = 37.8056o (1 1 1), 44.0345o (2 0 0), 64.3942o (2 2 0), dan 77.5003o (3 1 1) with face-centered cubic (FCC) crystal structure, and the average particle size was 22.5047 nm. SEM results showed that the nanoparticles have a non-uniform and irregular shape.","PeriodicalId":17811,"journal":{"name":"Jurnal Kimia Sains dan Aplikasi","volume":" ","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-07-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis of Silver Nanoparticles in an Eco-friendly Way using Lannea coromandelica Aqueous Bark Extract\",\"authors\":\"N. Azis, A. Wahab, A. Karim, N. La Nafie, Triana Febrianti\",\"doi\":\"10.14710/jksa.25.6.224-230\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this present study, silver nanoparticles (AgNPs) were synthesized through an easy, rapid, and eco-friendly pathway using Lannea coromandelica aqueous bark extract. The obtained AgNPs were characterized using Ultraviolet-Visible (UV-Vis) spectrophotometer, Fourier Transform Infrared (FTIR), X-ray Diffraction (XRD), and Scanning Electron Microscope (SEM). The results indicated that the pH of colloidal AgNPs played a vital role in forming AgNPs. The pH ranges used in this study were 6, 8, 10, and 12. The formation of AgNPs was confirmed by observing the surface plasmon resonance (SPR) band at each pH and obtaining a wavelength of 430.50, 419.50, 418.50, and 410.00 nm. A comparison of the FTIR spectra of Lannea coromandelica aqueous bark extract and AgNPs showed the contribution of the O-H group in reducing silver ions. XRD diffractogram showed that AgNPs formed at 2θ = 37.8056o (1 1 1), 44.0345o (2 0 0), 64.3942o (2 2 0), dan 77.5003o (3 1 1) with face-centered cubic (FCC) crystal structure, and the average particle size was 22.5047 nm. SEM results showed that the nanoparticles have a non-uniform and irregular shape.\",\"PeriodicalId\":17811,\"journal\":{\"name\":\"Jurnal Kimia Sains dan Aplikasi\",\"volume\":\" \",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-07-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Jurnal Kimia Sains dan Aplikasi\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.14710/jksa.25.6.224-230\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Jurnal Kimia Sains dan Aplikasi","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.14710/jksa.25.6.224-230","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

在本研究中,使用香兰水性树皮提取物,通过一种简单、快速、环保的途径合成了银纳米颗粒(AgNPs)。使用紫外-可见(UV-Vis)分光光度计、傅立叶变换红外(FTIR)、X射线衍射(XRD)和扫描电子显微镜(SEM)对所获得的AgNPs进行了表征。结果表明,胶体AgNPs的pH值在形成AgNPs中起着至关重要的作用。本研究中使用的pH值范围为6、8、10和12。通过在每个pH下观察表面等离子体共振(SPR)带并获得430.50、419.50、418.50和410.00nm的波长来确认AgNP的形成。对北美兰水性树皮提取物和AgNPs的FTIR光谱的比较显示了O-H基团在还原银离子方面的贡献。XRD衍射图显示,AgNPs在2θ=37.8056o(11 1)、44.0345o(2 0 0)、64.3942o(2 0)和77.5003o(3 1 1)处形成面心立方(FCC)晶体结构,平均粒径为22.5047nm。SEM结果表明,纳米颗粒具有不均匀和不规则的形状。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of Silver Nanoparticles in an Eco-friendly Way using Lannea coromandelica Aqueous Bark Extract
In this present study, silver nanoparticles (AgNPs) were synthesized through an easy, rapid, and eco-friendly pathway using Lannea coromandelica aqueous bark extract. The obtained AgNPs were characterized using Ultraviolet-Visible (UV-Vis) spectrophotometer, Fourier Transform Infrared (FTIR), X-ray Diffraction (XRD), and Scanning Electron Microscope (SEM). The results indicated that the pH of colloidal AgNPs played a vital role in forming AgNPs. The pH ranges used in this study were 6, 8, 10, and 12. The formation of AgNPs was confirmed by observing the surface plasmon resonance (SPR) band at each pH and obtaining a wavelength of 430.50, 419.50, 418.50, and 410.00 nm. A comparison of the FTIR spectra of Lannea coromandelica aqueous bark extract and AgNPs showed the contribution of the O-H group in reducing silver ions. XRD diffractogram showed that AgNPs formed at 2θ = 37.8056o (1 1 1), 44.0345o (2 0 0), 64.3942o (2 2 0), dan 77.5003o (3 1 1) with face-centered cubic (FCC) crystal structure, and the average particle size was 22.5047 nm. SEM results showed that the nanoparticles have a non-uniform and irregular shape.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
36
审稿时长
17 weeks
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信